[(2-溴苯基)甲基]三苯基-鏻溴化物合成路线 （共 15 条）
反应条件
in toluene
3 h; Heating;
参考文献
Hopf, Henning; Hucker, Joachim; Ernst, Ludger
European Journal of Organic Chemistry, 2007 , # 12 p. 1891 - 1904
反应条件
1: NBS / acetone / 6 h / Irradiation
2: dimethylformamide
View Scheme
参考文献
Terfort, Andreas; Brunner, Henri
Journal of the Chemical Society - Perkin Transactions 1, 1996 , # 12 p. 1467 - 1479
反应条件
1: sodium tetrahydroborate / methanol / 18 h / 20 °C
2: phosphorus tribromide / dichloromethane / 2 h / 20 °C
3: toluene / 144 h / |Reflux
View Scheme
参考文献
Bozinovic, Nina; Opsenica, Igor; Solaja, Bogdan A.
Synlett, 2013 , vol. 24, # 1 p. 49 - 52
反应条件
1: phosphorus tribromide / dichloromethane / 2 h / 20 °C
2: toluene / 144 h / |Reflux
View Scheme
参考文献
Bozinovic, Nina; Opsenica, Igor; Solaja, Bogdan A.
Synlett, 2013 , vol. 24, # 1 p. 49 - 52
反应条件
copper(l) iodide; 1,10-phenanthroline; potassium iodide in 1,4-dioxane
T=20 - 100°C; Wittig Olefination; 32.0833 h; Inert atmosphere;
参考文献
Yu, Hui; Zhang, Meishu; Li, Yuzhe
Journal of Organic Chemistry, 2013 , vol. 78, # 17 p. 8898 - 8903
反应条件
1: potassium tert-butylate / tetrahydrofuran / 5 h / |Schlenk technique
2: K2S; copper diacetate / N,N-dimethyl-formamide / 24 h / 140 °C / |Schlenk technique; |Inert atmosphere
View Scheme
参考文献
Zhang, Xiaoyun; Zeng, Weilan; Yang, Yuan; Huang, Hui; Liang, Yun
Synlett, 2013 , vol. 24, # 13 art. no. ST-2013-W0339-L, p. 1687 - 1692
反应条件
sodium ethanolate in ethanol
参考文献
Yu, Jie; Li, Nan; Chen, Dian-Feng; Luo, Shi-Wei
Tetrahedron Letters, 2014 , vol. 55, # 17 p. 2859 - 2864
反应条件
sodium ethanolate in ethanol
参考文献
Yu, Jie; Li, Nan; Chen, Dian-Feng; Luo, Shi-Wei
Tetrahedron Letters, 2014 , vol. 55, # 17 p. 2859 - 2864
反应条件
sodium methylate in methanol
16 h;
参考文献
Brouw, P. M. op den; Laarhoven, W. H.
Recueil: Journal of the Royal Netherlands Chemical Society, 1982 , vol. 101, # 2 p. 58 - 67
反应条件
sodium ethanolate in ethanol
Ambient temperature;
参考文献
Munro, David P.; Sharp, John T.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1984 , # 4 p. 849 - 858
