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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
2-(苯硫基)苯甲醛
合成路线
（共 26 条）
→
反应条件
36943-39-2
2-(苯硫基)苯甲醛
反应条件
palladium diacetate; N-ethyl-N,N-diisopropylamine; 9,9-dimethyl-4,5-bis(diphenyl-phosphino)xanthene in N,N-dimethyl-formamide T=100°C; 4 h; Inert atmosphere;
参考文献
Lee, Jae-Young; Phil, Ho Lee
Journal of Organic Chemistry, 2008 , vol. 73, # 18 p. 7413 - 7416
1527-14-6
2-(苯硫基)苄醇
→
反应条件
36943-39-2
2-(苯硫基)苯甲醛
反应条件
pyridinium chlorochromate in dichloromethane T=20°C; Oxidation; 4 h;
参考文献
Bonnet, B.Eatrice; Soullez, David; Girault, Sophie; Maes, Louis; Landry, Valerie; Davioud-Charvet, Elisabeth; Sergheraert, Christian
Bioorganic and Medicinal Chemistry, 2000 , vol. 8, # 1 p. 95 - 103
6630-33-7
邻溴苯甲醛
+
882-33-7
二苯二硫醚
→
反应条件
36943-39-2
2-(苯硫基)苯甲醛
反应条件
zinc; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride in tetrahydrofuran 24 h; Heating;
参考文献
Fukuzawa, Shin-Ichi; Tanihara, Daisuke; Kikuchi, Satoshi
Synlett, 2006 , # 13 p. 2145 - 2147
108-98-5
硫酚
+
552-89-6
邻硝基苯甲醛
→
反应条件
36943-39-2
2-(苯硫基)苯甲醛
反应条件
magnesium methanolate in N,N-dimethyl-formamide T=80°C; 4 h;
参考文献
Naeimi, Hossein; Moradian, Mohsen
Synlett, 2012 , vol. 23, # 15 p. 2223 - 2226
Title/Abstract Full Text View citing articles Show Details
Naeimi, Hossein; Moradian, Mohsen
Tetrahedron Asymmetry, 2014 , vol. 25, # 5 p. 429 - 434
→
反应条件
36943-39-2
2-(苯硫基)苯甲醛
反应条件
1: 2-chloro-benzaldehyde With palladium diacetate; 9,9-dimethyl-4,5-bis(diphenyl-phosphino)xanthene in N,N-dimethyl-formamide T=20°C; 0.0833333 h; Inert atmosphere; 2: In(SPh)3 With caesium carbonate in N,N-dimethyl-formamide T=100°C; 4 h; Inert atmosphere;
参考文献
Atobe, Shingo; Sonoda, Motohiro; Suzuki, Yuki; Shinohara, Hiroyuki; Yamamoto, Takuya; Ogawa, Akiya
Chemistry Letters, 2011 , vol. 40, # 9 p. 980 - 982
108-98-5
硫酚
+
6630-33-7
邻溴苯甲醛
→
反应条件
36943-39-2
2-(苯硫基)苯甲醛
反应条件
1.2.3.4-tetrahydro-8-hydroxy-quinoline; potassium carbonate; copper(I) bromide in dimethyl sulfoxide T=80°C; Ullmann reaction; 24 h; Inert atmosphere;
参考文献
Feng, Yang; Wang, Huifeng; Sun, Fangfang; Li, Yaming; Fu, Xinmei; Jin, Kun
Tetrahedron, 2009 , vol. 65, # 47 p. 9737 - 9741
108-98-5
硫酚
→
反应条件
36943-39-2
2-(苯硫基)苯甲醛
反应条件
potassium carbonate in N,N-dimethyl-formamide
参考文献
Zhang, Henry Q.; Xia, Zhiren; Kolasa, Teodozyj; Dinges, Jurgen
Tetrahedron Letters, 2003 , vol. 44, # 48 p. 8661 - 8663
88-67-5
邻碘苯甲酸
→
反应条件
36943-39-2
2-(苯硫基)苯甲醛
反应条件
1: 60 percent / KOH; copper / H2O / 12 h / Heating 2: 59 percent / BH3*THF / tetrahydrofuran / 12 h / 20 °C 3: 72 percent / pyridinium chlorochromate / CH2Cl2 / 4 h / 20 °C View Scheme
参考文献
Bonnet, B.Eatrice; Soullez, David; Girault, Sophie; Maes, Louis; Landry, Valerie; Davioud-Charvet, Elisabeth; Sergheraert, Christian
Bioorganic and Medicinal Chemistry, 2000 , vol. 8, # 1 p. 95 - 103
1527-12-4
2-(苯基硫代)苯甲酸
→
反应条件
36943-39-2
2-(苯硫基)苯甲醛
反应条件
1: 59 percent / BH3*THF / tetrahydrofuran / 12 h / 20 °C 2: 72 percent / pyridinium chlorochromate / CH2Cl2 / 4 h / 20 °C View Scheme
参考文献
Bonnet, B.Eatrice; Soullez, David; Girault, Sophie; Maes, Louis; Landry, Valerie; Davioud-Charvet, Elisabeth; Sergheraert, Christian
Bioorganic and Medicinal Chemistry, 2000 , vol. 8, # 1 p. 95 - 103
352427-08-8
→
反应条件
36943-39-2
2-(苯硫基)苯甲醛
+
91804-55-6
反应条件
in various solvent(s) 1 h; Heating;
参考文献
Leardini; McNab; Minozzi; Nanni
Journal of the Chemical Society. Perkin Transactions 1, 2001 , # 9 p. 1072 - 1078
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