乙基(2E)-3,4,4-三甲基-2-戊烯酸酯合成路线 （共 5 条）
反应条件
pyridine; thionyl chloride in diethyl ether
参考文献
DeBoer,A.; Hunter,J.A.
Journal of Organic Chemistry, 1973 , vol. 38, # 1 p. 144 - 146
反应条件
1,2-dimethyl-1H-imidazole in diethyl ether
T=21°C; Irradiation;
参考文献
Weedon
Canadian Journal of Chemistry, 1984 , vol. 62, # 10 p. 1933 - 1939
反应条件
1: 36 percent / Zn
2: 63 percent / N,N-dimethylaniline / CHCl3 / 9 h / Heating
3: potassium tert-butoxide / 2-methyl-propan-2-ol / 0.25 h
View Scheme
参考文献
Weedon
Canadian Journal of Chemistry, 1984 , vol. 62, # 10 p. 1933 - 1939
反应条件
potassium tert-butylate in tert-butyl alcohol
0.25 h; Yield given. Yields of byproduct given;
参考文献
Weedon
Canadian Journal of Chemistry, 1984 , vol. 62, # 10 p. 1933 - 1939
反应条件
1,2-dimethyl-1H-imidazole in diethyl ether
T=51°C; Irradiationwith 3,4-dimethyl derivatives, other products; other solvents, without base; Quantum yieldProduct distributionMechanism;
参考文献
Weedon
Canadian Journal of Chemistry, 1984 , vol. 62, # 10 p. 1933 - 1939
