1: 1.) LDA, 2.) TMSCl, 4.) aq. HCl 2: 99 percent / CeCl3*H2O, NaBH4 / methanol / 0.17 h 3: 93 percent / DMAP / CH2Cl2 / 24 h / Heating 4: tributyltin hydride, AIBN / benzene / 8 h / Heating View Scheme

1: 99 percent / CeCl3*H2O, NaBH4 / methanol / 0.17 h 2: 93 percent / DMAP / CH2Cl2 / 24 h / Heating 3: tributyltin hydride, AIBN / benzene / 8 h / Heating View Scheme

hexacarbonyl molybdenum in hexane 72 h;

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