三(2,2,2-三氟乙基)亚磷酸酯合成路线 （共 26 条）
反应条件
in benzene T=20 - 25°C; 2 h;
参考文献
Krutikova; Krutikov; Erkin
Russian Journal of General Chemistry, 2010 , vol. 80, # 3 p. 434 - 439
反应条件
T=185 - 195°C; 7 h; sealed glass tube;
参考文献
Maslennikov, I. G.; Kirichenko, L. N.; Garabadzhiu, A. V.; Koshcheeva, L. S.; Lavrent'ev, A. N.; Sochilin, E. G.
J. Gen. Chem. USSR (Engl. Transl.), 1980 , vol. 50, # 7 p. 1648 - 1650,1346 - 1348
参考文献
Mironov, V.F.; Sinyashina, T.N.; Ofitserov, E.N.; Konovalova, I.V.
Russian Journal of General Chemistry, 1994 , vol. 64, # 8.2 p. 1225 - 1227
Zhurnal Obshchei Khimii, 1994 , vol. 64, # 8 p. 1366 - 1368
反应条件
aluminum oxide; potassium fluoride in acetonitrile Arbuzov reaction; Heating;
参考文献
Fortin, Samuel; Dupont, Felix; Deslongchamps, Pierre
Journal of Organic Chemistry, 2002 , vol. 67, # 15 p. 5437 - 5439
反应条件
cyclohexane-1,2-epoxide UV-irradiation;
参考文献
Nalli, Thomas W.; Stanek, Lee G.; Molenaar, Rebekka H.; Weidell, Krysia L.; Meyer, Justin P.; Johnson, Brandon R.; Steckler, Timothy T.; Wackerly, Jay Wm.; Studler, Missy Jo; Vickerman, Kevin L.; Klankowski, Stephen A.
Journal of Organic Chemistry, 2013 , vol. 78, # 8 p. 3561 - 3569
参考文献
Lowther, Nicholas; Crook, Polly; Hall, C. Dennis
Phosphorus, Sulfur and Silicon and the Related Elements, 1995 , vol. 102, # 1-4 p. 195 - 204
反应条件
bromine; triethylamine in diethyl ether 1.) -50 deg to -60 deg C, 1.5 h, 2.) 20 deg C, 12 h;
参考文献
Mironov; Bredikhin; Bredikhina; Novikova; Konovalova
Russian Journal of General Chemistry, 1997 , vol. 67, # 8 p. 1204 - 1207
反应条件
cyclohexane-1,2-epoxide in neat (no solvent) T=34°C; 4.16667 h; UV-irradiation;
参考文献
Nalli, Thomas W.; Stanek, Lee G.; Molenaar, Rebekka H.; Weidell, Krysia L.; Meyer, Justin P.; Johnson, Brandon R.; Steckler, Timothy T.; Wackerly, Jay Wm.; Studler, Missy Jo; Vickerman, Kevin L.; Klankowski, Stephen A.
Journal of Organic Chemistry, 2013 , vol. 78, # 8 p. 3561 - 3569
反应条件
cyclohexane-1,2-epoxide in acetonitrile-D3 T=34°C; 4.5 h; UV-irradiation;
参考文献
Nalli, Thomas W.; Stanek, Lee G.; Molenaar, Rebekka H.; Weidell, Krysia L.; Meyer, Justin P.; Johnson, Brandon R.; Steckler, Timothy T.; Wackerly, Jay Wm.; Studler, Missy Jo; Vickerman, Kevin L.; Klankowski, Stephen A.
Journal of Organic Chemistry, 2013 , vol. 78, # 8 p. 3561 - 3569
反应条件
chloral T=20°C; 72 h;
参考文献
Mironov, V.F.; Sinyashina, T.N.; Ofitserov, E.N.; Konovalova, I.V.
Russian Journal of General Chemistry, 1994 , vol. 64, # 8.2 p. 1225 - 1227
Zhurnal Obshchei Khimii, 1994 , vol. 64, # 8 p. 1366 - 1368
