2-二乙氧基硫代膦酰硫基丁二酸二乙基酯合成路线 (共 3 条)
反应条件
1: methanol; ethanol With diphosphorus pentasulfide in toluene
T=70°C;
2: maleic acid diethyl ester With hydroquinone in water
T=55°C; 5 h;
参考文献
Gutman, Daniella; Baidossi, Wael
Patent: US2007/10496 A1, 2007 ;
Location in patent: Page/Page column 13 ;
反应条件
triethylamine; hydroquinone
参考文献
Mel'nikow; Schwezowa-Schilowskaja
Zhurnal Obshchei Khimii, 1953 , vol. 23, p. 1352,1356;engl.Ausg.S.1417,1420
Full Text Show Details
Am.Cyanamid Co.
Patent: DE847897 , 1951 ;
Full Text Show Details
Am.Cyanamid Co.
Patent: US2578652 , 1950 ;
DRP/DRBP Org.Chem.
参考文献
Pudovik,A.N.; Cherkasov,R.A.
J. Gen. Chem. USSR (Engl. Transl.), 1968 , vol. 38, # 11 p. 2532 - 2538,2448 - 2452