1-(2,2-二氯乙烯基)吡咯烷-2-酮合成路线 （共 6 条）
反应条件
N(Et)4ClO4 in N,N-dimethyl-formamide
T=20°C; electroreduction: mercury pool cathode; working potential 1.5 V (versus SCE);
参考文献
Casadei, Maria Antonietta; Cesa, Stefania; Moracci, Franco Micheletti; Inesi, Achille
Gazzetta Chimica Italiana, 1993 , vol. 123, # 8 p. 457 - 462
反应条件
N(Et)4ClO4 in N,N-dimethyl-formamide
T=20°C; electroreduction: mercury pool cathode; working potential 1.6 V (versus SCE);
参考文献
Casadei, Maria Antonietta; Cesa, Stefania; Moracci, Franco Micheletti; Inesi, Achille
Gazzetta Chimica Italiana, 1993 , vol. 123, # 8 p. 457 - 462
反应条件
N(Et)4ClO4 in N,N-dimethyl-formamide
T=20°C; electrochem. reduction on a Hg-cathode, -1,5 V, current 0.2 A to 10 mA;
参考文献
Casadei, M. A.; Inesi, A.
Bulletin de la Societe Chimique de France, 1991 , # 1 p. 54 - 60
反应条件
anhydrous tetraethylammonium acetate; N(Et)4ClO4 in N,N-dimethyl-formamide
1 h; Ambient temperature; Yield given;
参考文献
Casadei, M. A.; Inesi, A.
Bulletin de la Societe Chimique de France, 1991 , # 1 p. 54 - 60
反应条件
1: 70 percent / SOCl2 / 2 h / Heating
2: 70 percent / tetraethylammonium perchlorate / dimethylformamide / 20 °C / electroreduction: mercury pool cathode; working potential 1.5 V (versus SCE)
View Scheme
参考文献
Casadei, Maria Antonietta; Cesa, Stefania; Moracci, Franco Micheletti; Inesi, Achille
Gazzetta Chimica Italiana, 1993 , vol. 123, # 8 p. 457 - 462
反应条件
anhydrous tetraethylammonium acetate; N(Et)4ClO4 in N,N-dimethyl-formamide
1 h; Ambient temperature; Yield given;
参考文献
Casadei, M. A.; Inesi, A.
Bulletin de la Societe Chimique de France, 1991 , # 1 p. 54 - 60
