N-苯甲酰基-D-苯丙氨酸合成路线 （共 30 条）
反应条件
tri-cyclo-hexyl-phosphine; [RhCl(η2:η2-cycloocta-1,5-diene)]2 in acetonitrile T=60°C; Racemization; 48 h;
参考文献
Hateley, Martin J.; Schichl, Daniel A.; Kreuzfeld, Hans-Joern; Beller, Matthias
Tetrahedron Letters, 2000 , vol. 41, # 20 p. 3821 - 3824
反应条件
sodium amalgam; water
参考文献
Lamb; Robson
Biochemical Journal, 1931 , vol. 25, p. 1231,1235
反应条件
water in various solvent(s) T=50°C; 35 h; Pseudomonas cepacia lipase; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Crich, Joyce Z.; Brieva, Rosario; Marquart, Peer; Gu, Rui-Lin; Flemming, Steffen; Sih, Charles J.
Journal of Organic Chemistry, 1993 , vol. 58, # 12 p. 3252 - 3258
反应条件
Candida antarctica lipase B cross-linked crystal; triethylamine in water; toluene T=37°C; 4 h; Title compound not separated from byproducts.;
参考文献
Quiros; Parker; Turner
Journal of Organic Chemistry, 2001 , vol. 66, # 15 p. 5074 - 5079
反应条件
1: 75 percent / ethyl acetate / 2 h 2: 280 mg / H2 / 1 percent PdCl2 / ethanol / 10 h 3: 10 percent NaOH / 4 h 4: 58 percent / pyridine / 1 h / 90 °C 5: 3 percent KOH / ethanol / 1 h / Heating View Scheme
参考文献
Noguchi; Mochida; Shingu; et al.
Chemical and Pharmaceutical Bulletin, 1984 , vol. 32, # 9 p. 3584 - 3587
反应条件
1: 280 mg / H2 / 1 percent PdCl2 / ethanol / 10 h 2: 10 percent NaOH / 4 h 3: 58 percent / pyridine / 1 h / 90 °C 4: 3 percent KOH / ethanol / 1 h / Heating View Scheme
参考文献
Noguchi; Mochida; Shingu; et al.
Chemical and Pharmaceutical Bulletin, 1984 , vol. 32, # 9 p. 3584 - 3587
反应条件
potassium hydroxide; zinc 1 h; Heating;
参考文献
Devasia, Ganapathiplackal M.; Shafi, P. Mohamed
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1986 , vol. 25, p. 204 - 206
反应条件
18-crown-6 ether in benzene 24 h;
参考文献
Muneer, Mohammed; Tikare, Ravindra K.; Kamat, Prashant V.; George, Manapurathu V.
Canadian Journal of Chemistry, 1987 , vol. 65, p. 1624 - 1630
反应条件
trifluoroacetic acid 0.5 h;
参考文献
Shanahan, Stephen E.; Byrne, Douglas D.; Inglis, Graham G. A.; Alam, Mahbub; Macdonald, Simon J. F.
Chemical Communications, 2002 , # 21 p. 2554 - 2555
反应条件
1: Et3N / 0.17 h / 20 °C 2: CF3CO2H / 0.5 h View Scheme
参考文献
Shanahan, Stephen E.; Byrne, Douglas D.; Inglis, Graham G. A.; Alam, Mahbub; Macdonald, Simon J. F.
Chemical Communications, 2002 , # 21 p. 2554 - 2555
