(-)-二甲基-2,3-邻异丙亚基-L-酒石酸酯合成路线 (共 28 条)
参考文献
Seebach, Dieter; Beck, Albert K.; Imwinkelried, Rene; Roggo, Silvio; Wonnacott, Anne
Helvetica Chimica Acta, 1987 , vol. 70, p. 954 - 974
反应条件
hydrogenchloride in water; N,N-dimethyl-formamide; orthoformic acid triethyl ester T=20°C; 72 h;
参考文献
Magee, David I.; Silk, Peter J.; Wu, Junping; Mayo, Peter D.; Ryall, Krista
Tetrahedron, 2011 , vol. 67, # 29 p. 5329 - 5338
反应条件
toluene-4-sulfonic acid in methanol 5 h; HeatingInert atmosphere;
参考文献
Kobayashi, Yuka; Kokubo, Yasushi; Aisaka, Takamitsu; Saigo, Kazuhiko
Tetrahedron Asymmetry, 2008 , vol. 19, # 21 p. 2536 - 2541
反应条件
toluene-4-sulfonic acid T=85 - 95°C;
参考文献
Velthuisen, Emile J.; Baughman, Todd M.; Johns, Brian A.; Temelkoff, David P.; Weatherhead, Jason G.
European Journal of Medicinal Chemistry, 2013 , vol. 63, p. 202 - 212
反应条件
1: With toluene-4-sulfonic acid Heating; 2: in cyclohexane Heating;
参考文献
Li, Baohua; Yang, Xuemei; Yang, Kai; Fu, Enqin
Synthetic Communications, 2005 , vol. 35, # 19 p. 2603 - 2608
反应条件
toluene-4-sulfonic acid in benzene 8 h; RefluxInert atmosphereDean-Stark;
参考文献
Zou, Liwei; Wang, Baomin; Mu, Hongfang; Zhang, Huanrui; Song, Yuming; Qu, Jingping
Organic Letters, 2013 , vol. 15, # 12 p. 3106 - 3109
反应条件
camphor-10-sulfonic acid in tetrahydrofuran T=20°C; 8 h; Inert atmosphere;
参考文献
Khan, Sher Wali; Zaidi, Javed Hussain; Yousuf, Sammer; Khan, Khalid Mohammed; Ambreen, Nida; Khan, Momin; Perveen, Shahnaz; Miana, Ghulam Abbas
Journal of the Chemical Society of Pakistan, 2013 , vol. 35, # 3 p. 875 - 885
反应条件
ruthenium(IV) oxide; sodium periodate in water; acetone
参考文献
Barton, Derek H. R.; Gateau-Olesker, Alice; Gero, Stephan D.; Lacher, Brigitte; Tachdjian, Catherine; Zard, Samir Z.
Journal of the Chemical Society, Chemical Communications, 1987 , p. 1790 - 1792
反应条件
in diethyl ether; acetonitrile 0.5 h; Ambient temperature; Yield given;
参考文献
Barton; Gateau-Olesker; Gero; Lacher; Tachdjian; Zard
Tetrahedron, 1993 , vol. 49, # 21 p. 4589 - 4602
反应条件
chloro-trimethyl-silane; 2,2-dimethoxy-propane 24 h; Ambient temperature;
参考文献
Rodriguez; Nomen; Spur; Godfroid
Tetrahedron Letters, 1998 , vol. 39, # 47 p. 8563 - 8566