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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
3704-40-3
合成路线
（共 44 条）
1826-13-7
5-苯基噻唑
+
591-50-4
碘苯
→
反应条件
3704-40-3
反应条件
dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II) dichloromethane adduct; triphenylphosphine; silver carbonate in water T=60°C; 24 h; regioselective reaction;
参考文献
Tani, Satoshi; Uehara, Takahiro N.; Yamaguchi, Junichiro; Itami, Kenichiro
Chemical Science, 2013 , vol. 5, # 1 p. 123 - 135
288-47-1
噻唑
+
108-86-1
溴代苯
→
反应条件
3704-40-3
反应条件
palladium diacetate; caesium carbonate; biphenyl-2-yl-di-tert-butyl-phosphane in N,N-dimethyl-formamide T=150°C; 3 h;
参考文献
Yokooji, Aya; Okazawa, Toru; Satoh, Tetsuya; Miura, Masahiro; Nomura, Masakatsu
Tetrahedron, 2003 , vol. 59, # 30 p. 5685 - 5689
108-86-1
溴代苯
→
反应条件
3704-40-3
反应条件
tetrakis(triphenylphosphine) palladium(0); caesium carbonate in 1,4-dioxane T=170°C; Suzuki-Miyaura cross-coupling; 0.333333 h; Microwave irradiation;
参考文献
Haemmerle, Johanna; Schnuerch, Michael; Iqbal, Naseer; Mihovilovic, Marko D.; Stanetty, Peter
Tetrahedron, 2010 , vol. 66, # 40 p. 8051 - 8059
591-50-4
碘苯
→
反应条件
3704-40-3
反应条件
tetrakis(triphenylphosphine) palladium(0); caesium carbonate in 1,4-dioxane T=170°C; Suzuki-Miyaura cross-coupling; 0.333333 h; Microwave irradiation;
参考文献
Haemmerle, Johanna; Schnuerch, Michael; Iqbal, Naseer; Mihovilovic, Marko D.; Stanetty, Peter
Tetrahedron, 2010 , vol. 66, # 40 p. 8051 - 8059
1000029-07-1
+
24388-23-6
苯硼酸频哪醇酯
→
反应条件
3704-40-3
反应条件
tetrakis(triphenylphosphine) palladium(0); potassium carbonate in N,N-dimethyl-formamide T=110°C; Suzuki-Miyaura coupling; 21 h;
参考文献
Haemmerle, Johanna; Schnuerch, Michael; Iqbal, Naseer; Mihovilovic, Marko D.; Stanetty, Peter
Tetrahedron, 2010 , vol. 66, # 40 p. 8051 - 8059
53715-67-6
5-溴-2-苯基-1,3-噻唑
+
24388-23-6
苯硼酸频哪醇酯
→
反应条件
3704-40-3
反应条件
tetrakis(triphenylphosphine) palladium(0); potassium carbonate in N,N-dimethyl-formamide T=110°C; Suzuki-Miyaura coupling; 16 h;
参考文献
Haemmerle, Johanna; Schnuerch, Michael; Iqbal, Naseer; Mihovilovic, Marko D.; Stanetty, Peter
Tetrahedron, 2010 , vol. 66, # 40 p. 8051 - 8059
1826-11-5
2-苯基噻唑
+
98-80-6
苯硼酸
→
反应条件
3704-40-3
反应条件
lithium boron tetrafluoride; 1,10-phenanthroline; 2,2,6,6-tetramethyl-1-piperidinyloxy, free radical; palladium diacetate in N,N-dimethyl acetamide T=100°C; 24 h; Reagent/catalystConcentration; Overall yield = 93 percent; regioselective reaction;
参考文献
Tani, Satoshi; Uehara, Takahiro N.; Yamaguchi, Junichiro; Itami, Kenichiro
Chemical Science, 2013 , vol. 5, # 1 p. 123 - 135
425392-56-9
→
反应条件
3704-40-3
反应条件
in water; N,N-dimethyl-formamide T=150°C; 18 h;
参考文献
Hodgetts, Kevin J.; Kershaw, Mark T.
Organic Letters, 2002 , vol. 4, # 8 p. 1363 - 1365
125877-36-3
→
反应条件
3704-40-3
反应条件
sodium hydroxide; SCl2 in dichloromethane 1 h; Ambient temperature;
参考文献
Komatsu, Mitsuo; Ohshiro, Yoshiki; Agawa, Toshio
Heterocycles, 1984 , vol. 21, # 2 p. 623
1000029-07-1
+
960-16-7
三丁基苯基锡
→
反应条件
3704-40-3
反应条件
cesium fluoride; tetrakis(triphenylphosphine) palladium(0) in toluene Stille cross-coupling reaction; Heating;
参考文献
Haemmerle, Johanna; Schnuerch, Michael; Iqbal, Naseer; Mihovilovic, Marko D.; Stanetty, Peter
Tetrahedron, 2010 , vol. 66, # 40 p. 8051 - 8059
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