二甲基-二(三甲基硅烷基)硅烷合成路线 (共 28 条)
反应条件
18 h; Heating; Product distributionMechanism;
参考文献
Chesnokova, T. A.; Kornev, A. N.; Semenov, V. V.; Kurskii, Yu. A.; Razuvaev, G. A.
J. Gen. Chem. USSR (Engl. Transl.), 1989 , vol. 59, # 5.1 p. 1057 - 1062,934 - 937
反应条件
boron trichloride in chloroform-d1
T=100°C; 48 h; ampoule;
参考文献
Einholz, Wolfgang; Gollinger, Walter; Haubold, Wolfgang
Zeitschrift fuer Naturforschung, B: Chemical Sciences, 1990 , vol. 45, # 1 p. 25 - 30
反应条件
boron trichloride in chloroform-d1
T=140°C; 16 h; ampoule;
参考文献
Einholz, Wolfgang; Gollinger, Walter; Haubold, Wolfgang
Zeitschrift fuer Naturforschung, B: Chemical Sciences, 1990 , vol. 45, # 1 p. 25 - 30
反应条件
chloro-trimethyl-silane; aluminium trichloride
Heating;
参考文献
Hengge, E.; Eibl, M.; Stadelmann, B.
Monatshefte fuer Chemie, 1993 , vol. 124, # 5 p. 523 - 528
反应条件
boron trichloride in chloroform-d1
T=140°C; 16 h; ampoule;
参考文献
Einholz, Wolfgang; Gollinger, Walter; Haubold, Wolfgang
Zeitschrift fuer Naturforschung, B: Chemical Sciences, 1990 , vol. 45, # 1 p. 25 - 30
反应条件
hydrogenchloride; tetrabutyl ammonium fluoride
1.) THF, HMPA, room temperature; 2.) methanol; Yield given. Multistep reaction;
参考文献
Hiyama, Tamejiro; Obayashi, Michio
Tetrahedron Letters, 1983 , vol. 24, # 38 p. 4109 - 4112
反应条件
tetrabutyl ammonium fluoride in N,N,N',N',N'',N''-hexamethylphosphoric triamide
tetrabutylammonium fluoride was added to an HMPA solution of octatmethyltrisilane and butadiene;
参考文献
Hiyama, Tamejiro; Obayashi, Michio
Tetrahedron Letters, 1983 , vol. 24, # 38 p. 4109 - 4112
反应条件
tetrabutyl ammonium fluoride in N,N,N',N',N'',N''-hexamethylphosphoric triamide
octamethyltrisilane added to an HMPA solution of butadiene and tetrabutylammonium fluoride;
参考文献
Hiyama, Tamejiro; Obayashi, Michio
Tetrahedron Letters, 1983 , vol. 24, # 38 p. 4109 - 4112
反应条件
tetrabutyl ammonium fluoride in N,N,N',N',N'',N''-hexamethylphosphoric triamide
octamethyltrisilane added to an HMPA solution of butadiene and tetrabutylammonium fluoride;
参考文献
Hiyama, Tamejiro; Obayashi, Michio
Tetrahedron Letters, 1983 , vol. 24, # 38 p. 4109 - 4112
反应条件
tetrabutyl ammonium fluoride in N,N,N',N',N'',N''-hexamethylphosphoric triamide
参考文献
Hiyama, Tamejiro; Obayashi, Michio
Tetrahedron Letters, 1983 , vol. 24, # 38 p. 4109 - 4112