反应条件
in acetone
byproducts: Cl3CC(O)OH; to soln. of Ge complex (1.349 mmol) added concd. HCl, stirred under N2 at 50°C for 18 h; D. Simon et al., J. Organomet. Chem. 267 (1984) 133-142; cooled to -28°C, crystals washed with hexane/acetone (1:1), recrystd. from Et2O/hexane (2:1);
参考文献
Amadoruge, Monika L.; Short, Erin K.; Moore, Curtis; Rheingold, Arnold L.; Weinert, Charles S.
Journal of Organometallic Chemistry, 2010 , vol. 695, # 14 p. 1813 - 1823
