反应条件
1: 1-[4-(2-chloroethoxy)phenyl]-1-(4-iodophenyl)methanone; 1-phenyl-propan-1-one With titanium tetrachloride; 1,2-bis-(diphenylphosphino)ethane; zinc in 1,4-dioxane T=20°C; 2.5 h; Inert atmosphereReflux; 2: pyrrolidine in ethanol McMurry Reaction; 18 h; RefluxInert atmosphere;
参考文献
Ace, Karl W.; Armitage, Mark A.; Bellingham, Richard K.; Blackler, Paul D.; Ennis, David S.; Hussain, Nigel; Lathbury, David C.; Morgan, David O.; O'Connor, Noah; Oakes, Graham H.; Passey, Stephen C.; Powling, Laurence C.
Organic Process Research and Development, 2001 , vol. 5, # 5 p. 479 - 490