5,10,15,20-四(2,6-二氯苯基)卟啉合成路线 （共 16 条）
反应条件
1: With Tulsion-63 resin; 1,1,1-triethoxyethane in dichloromethane T=20°C; 17 h; 2: With chloranil in dichloromethane 2 h; Heating;
参考文献
Naik, Rajan; Joshi, Padmakar; Kaiwar, Sharada P.; Deshpande, Rajesh K.
Tetrahedron, 2003 , vol. 59, # 13 p. 2207 - 2213
反应条件
1: BF3 etherate / CHCl3 / Ambient temperature 2: Et3N, 35 w/vpercent H2O2, AcOH / 1 h / 20 - 30 °C View Scheme
参考文献
Li, Feirong; Yang, Kexin; Tyhonas, John S.; MacCrum, Kristy A.; Lindsey, Jonathan S.
Tetrahedron, 1997 , vol. 53, # 37 p. 12339 - 12360
反应条件
1: With Indion-130 resin in dichloromethane T=25°C; 17 h; 2: With chloranil in dichloromethane 3 h; Heating;
参考文献
Naik, Rajan; Joshi, Padmakar; Kaiwar, Sharada P.; Deshpande, Rajesh K.
Tetrahedron, 2003 , vol. 59, # 13 p. 2207 - 2213
反应条件
1: With methanesulfonic acid in dichloromethane T=20°C; 2 h; 2: With 2,3-dicyano-5,6-dichloro-p-benzoquinone
参考文献
Taniguchi, Ryuichiro; Shimizu, Soji; Suzuki, Masaaki; Shin, Ji-Young; Furuta, Hiroyuki; Osuka, Atsuhiro
Tetrahedron Letters, 2003 , vol. 44, # 12 p. 2505 - 2507
反应条件
1: With H(COOEt)3; boron trifluoride diethyl etherate in chloroform T=20°C; Condensation; 1.25 h; 2: With 2,3-dicyano-5,6-dichloro-p-benzoquinone in chloroform Oxidation;
参考文献
Assis, Marilda Das Dores; Lindsay Smith, John R.
Journal of the Chemical Society. Perkin Transactions 2, 1998 , # 10 p. 2221 - 2226
反应条件
1: With methanesulfonic acid in dichloromethane T=0°C; 2 h; 2: With 2,3-dicyano-5,6-dichloro-p-benzoquinone
参考文献
Taniguchi, Ryuichiro; Shimizu, Soji; Suzuki, Masaaki; Shin, Ji-Young; Furuta, Hiroyuki; Osuka, Atsuhiro
Tetrahedron Letters, 2003 , vol. 44, # 12 p. 2505 - 2507
反应条件
acetic anhydride; acetic acid in nitrobenzene T=120°C; 2 h;
参考文献
Mendes, Sonia; Camacho, Fabio; Silva, Tito; Calado, Cecilia R. C.; Serra, Armenio Coimbra; Rocha Gonsalves, Antonio M. D'A.; Roxo-Rosa, Monica
Photochemistry and Photobiology, 2011 , vol. 87, # 6 p. 1395 - 1404
反应条件
acetic acid; nitrobenzene T=120°C;
参考文献
Gonsalves, A. M. d'A.; Varejao, Jorge M. T. B.; Pereira, Mariette M.
Journal of Heterocyclic Chemistry, 1991 , vol. 28, # 3 p. 635 - 640
反应条件
1: dihydrogen peroxide / water; acetonitrile / 10 h / 25 °C / UV-irradiation 2: boron trifluoride diethyl etherate / dichloromethane / 20 °C / Inert atmosphere; Darkness 3: chloranil / dichloromethane / 20 °C / Reflux; Inert atmosphere; Darkness View Scheme
参考文献
Farhadi, Saeid; Zabardasti, Abedien; Rahmati, Mohammad Hosien
Journal of Chemical Research, 2011 , vol. 35, # 3 p. 157 - 160
反应条件
boron trifluoride diethyl etherate; 2,3-dicyano-5,6-dichloro-p-benzoquinone 1.) CH2Cl2, room temp., 15 h, 2.) CH2Cl2, room temp., 2 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Banfi, Stefano; Montanari, Fernando; Pozzi, Gianluca; Quici, Silvio
Tetrahedron, 1994 , vol. 50, # 30 p. 9025 - 9036
