2-氯-1,3-二甲基氯化咪唑啉合成路线 （共 25 条）
反应条件
phosgene in toluene T=0 - 40°C;
参考文献
Herres-Pawlis, Sonja; Floerke, Ulrich; Henkel, Gerald
European Journal of Inorganic Chemistry, 2005 , # 19 p. 3815 - 3824
反应条件
Mes3SiCl in toluene T=-60°C; 16 h; Irradiation;
参考文献
Neumann, Wilhelm P.; Schultz, Klaus-Dieter; Vieler, Robert
Journal of Organometallic Chemistry, 1984 , vol. 264, # 1-2 p. 179 - 192
反应条件
1,3,1',3'-tetramethyl-1,3,1',3'-tetrahydro-[2,2']biimidazolylidene in toluene T=-60°C; 16 h; Irradiation;
参考文献
Neumann, Wilhelm P.; Schultz, Klaus-Dieter; Vieler, Robert
Journal of Organometallic Chemistry, 1984 , vol. 264, # 1-2 p. 179 - 192
反应条件
in toluene T=20 - 60°C; 14 h;
参考文献
Raab, Volker; Harms, Klaus; Sundermeyer, Joerg; Kovacevic, Borislav; Maksic, Zvonimir B.
Journal of Organic Chemistry, 2003 , vol. 68, # 23 p. 8790 - 8797
反应条件
in 1,2-dichloro-ethane T=70°C; 3 h;
参考文献
Hamed, Atef; Mueller, Edgar; Jochims, Johannes C.
Tetrahedron, 1986 , vol. 42, # 24 p. 6645 - 6656
反应条件
in toluene Irradiation (UV/VIS); a soln. of chlorogermane and diimidazolidine irradiating for 20 h at -55°C, cold MeOH adding, digermane ppt. sepg., washing with cold MeOH under Ar, drying in vacuo at room temp.; identified by elem. anal., IR, UV, NMR and mass spectra;
参考文献
Neumann, Wilhelm P.; Schultz, Klaus-Dieter; Vieler, Robert
Journal of Organometallic Chemistry, 1984 , vol. 264, # 1-2 p. 179 - 192
反应条件
in toluene Irradiation (UV/VIS); a soln. of chlorogermane and diimidazolidine irradiating for 20 h at -60°C, cold MeOH adding, digermane ppt. sepg., washing with cold MeOH under Ar, drying in vacuo at room temp.; identified by elem. anal., IR, NMR and mass spectra;
参考文献
Neumann, Wilhelm P.; Schultz, Klaus-Dieter; Vieler, Robert
Journal of Organometallic Chemistry, 1984 , vol. 264, # 1-2 p. 179 - 192
反应条件
in toluene Irradiation (UV/VIS); a soln. of chlorogermane and diimidazolidine irradiating for 20 h at -60°C, cold MeOH adding, digermane ppt. sepg., washing with cold MeOH under Ar, drying in vacuo at room temp.; identified by elem. anal., IR, UV, NMR and mass spectra;
参考文献
Neumann, Wilhelm P.; Schultz, Klaus-Dieter; Vieler, Robert
Journal of Organometallic Chemistry, 1984 , vol. 264, # 1-2 p. 179 - 192
反应条件
in toluene Irradiation (UV/VIS); a soln. of chlorogermane and diimidazolidine irradiating for 20 h at -60°C, cold MeOH adding, digermane ppt. sepg., washing with cold MeOH under Ar, drying in vacuo at room temp.; identified by elem. anal., IR, UV, NMR and mass spectra;
参考文献
Neumann, Wilhelm P.; Schultz, Klaus-Dieter; Vieler, Robert
Journal of Organometallic Chemistry, 1984 , vol. 264, # 1-2 p. 179 - 192
反应条件
in toluene Irradiation (UV/VIS); a soln. of chlorogermane and diimidazolidine irradiating for 20 h at -70°C, cold MeOH adding, digermane ppt. sepg., washing with cold MeOH under Ar, drying in vacuo at room temp.; identified by elem. anal., IR, UV, NMR and mass spectra;
参考文献
Neumann, Wilhelm P.; Schultz, Klaus-Dieter; Vieler, Robert
Journal of Organometallic Chemistry, 1984 , vol. 264, # 1-2 p. 179 - 192
