2-氯-1,3-二甲基氯化咪唑啉合成路线 （共 25 条）
反应条件
in toluene Irradiation (UV/VIS); a soln. of chlorogermane and diimidazolidine irradiating for 20 h at room temp., MeOH adding, digermane ppt. sepg., washing with cold MeOH under Ar, drying in vacuo at room temp.; identified by elem. anal., IR, NMR and mass spectra;
参考文献
Neumann, Wilhelm P.; Schultz, Klaus-Dieter; Vieler, Robert
Journal of Organometallic Chemistry, 1984 , vol. 264, # 1-2 p. 179 - 192
参考文献
Mitsui Toatsu Chemicals, Inc.
Patent: US5750779 A1, 1998 ;
参考文献
Mitsui Toatsu Chemicals, Inc.
Patent: US5750779 A1, 1998 ;
反应条件
1: With triethylamine in acetonitrile Inert atmosphereReflux; 2: With sodium hydroxide in acetonitrile 1 h;
参考文献
Garnier, Jean; Kennedy, Alan R.; Berlouis, Leonard E. A.; Murphy, John A.; Turner, Andrew T.
Beilstein Journal of Organic Chemistry, 2010 , vol. 6, art. no. 73
反应条件
toluene-4-sulfonic acid in toluene
参考文献
Mitsui Toatsu Chemicals, Inc.
Patent: US5750779 A1, 1998 ;
反应条件
in tetrahydrofuran; hexanes T=-78°C; 1 h; Inert atmosphere;
参考文献
Snead, David R.; Ghiviriga, Ion; Abboud, Khalil A.; Hong, Sukwon
Organic Letters, 2009 , vol. 11, # 15 p. 3274 - 3277
参考文献
Mitsui Toatsu Chemicals, Inc.
Patent: US5750779 A1, 1998 ;
反应条件
triethylamine in methanol 1 h; Ambient temperature;
参考文献
Okawa, Tomohiro; Osakada, Naoto; Eguchi, Shoji; Kakehi, Akikazu
Tetrahedron, 1997 , vol. 53, # 47 p. 16061 - 16082
