5,10,15,20-四(4-氟苯基)-21H,23H-卟啉合成路线 （共 4 条）
反应条件
1: With Tulsion-63 resin; 1,1,1-triethoxyethane in dichloromethane
T=20°C; 17 h;
2: With chloranil in dichloromethane
2 h; Heating;
参考文献
Naik, Rajan; Joshi, Padmakar; Kaiwar, Sharada P.; Deshpande, Rajesh K.
Tetrahedron, 2003 , vol. 59, # 13 p. 2207 - 2213
反应条件
1: With Indion-130 resin in dichloromethane
T=25°C; 17 h;
2: With chloranil in dichloromethane
3 h; Heating;
参考文献
Naik, Rajan; Joshi, Padmakar; Kaiwar, Sharada P.; Deshpande, Rajesh K.
Tetrahedron, 2003 , vol. 59, # 13 p. 2207 - 2213
反应条件
1.1: 77 percent / Tulsion T-63 resin / 10 h / 20 °C
2.1: Indion-130 resin / CH2Cl2 / 17 h / 25 °C
2.2: 19 percent / p-chloranil / CH2Cl2 / 3 h / Heating
View Scheme
参考文献
Naik, Rajan; Joshi, Padmakar; Kaiwar, Sharada P.; Deshpande, Rajesh K.
Tetrahedron, 2003 , vol. 59, # 13 p. 2207 - 2213
反应条件
tetrafluoroboric acid; copper; sodium nitrite
1)H2O,5 deg C, 2) 100 deg C; Yield given. Multistep reaction;
参考文献
Semeikin, A.S.; Koifman, O.I.; Berezin, B.D.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1986 , vol. 22, # 4 p. 397 - 401
Khimiya Geterotsiklicheskikh Soedinenii, 1986 , vol. 22, # 4 p. 486 - 490
