in not given byproducts: Hg, C3F6; absence of air and moisture; heating of Hg-compd. with slight excess of Sn-compd. (sealed tube, 75°C, 1 week); product mixt. not sepd., detd. by (1)H-NMR spectroscopy;
参考文献
Eujen, Reint; Lagow, Richard J.
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), 1978 , p. 541 - 544
in benzene byproducts: perfluorocyclopropane; absence of air and moisture; heating of Ge-compd. 2 equiv. of Hg-compd. (sealed tube, 125°C, 3 weeks); not isolated, detd. by (19)F-NMR spectroscopy;
参考文献
Eujen, Reint; Lagow, Richard J.
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), 1978 , p. 541 - 544
in benzene byproducts: perfluorocyclopropane; absence of air and moisture; heating of Sn-compd. 2 equiv. of Hg-compd. (sealed tube, 125°C, 3 weeks); not isolated, detd. by (19)F-NMR spectroscopy;
参考文献
Eujen, Reint; Lagow, Richard J.
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), 1978 , p. 541 - 544
in benzene byproducts: perfluorocyclopropane; absence of air and moisture; heating of Pb-compd. 2 equiv. of Hg-compd. (sealed tube, 125°C, 3 weeks); not isolated, detd. by (19)F-NMR spectroscopy;
参考文献
Eujen, Reint; Lagow, Richard J.
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), 1978 , p. 541 - 544
