三氟-(三氟甲基硫基)甲烷合成路线 (共 58 条)
反应条件
sulfur(IV) fluoride
T=200°C;
参考文献
Middleton,W.J. et al.
Journal of Organic Chemistry, 1965 , vol. 30, p. 1375 - 1384
反应条件
sulfur; potassium fluoride; o-di-fluorobenzene in N,N-dimethyl-formamide
T=20°C; 0.166667 h;
参考文献
Chen, Chao; Chu, Lingling; Qing, Feng-Ling
Journal of the American Chemical Society, 2012 , vol. 134, # 30 p. 12454 - 12457
参考文献
Haas,A.; Oh,D.Y.
Chemische Berichte, 1969 , vol. 102, p. 77 - 82
反应条件
in Pyrex vessel at 25°C, unidentified products also formed;
参考文献
Kumar, Ramesh C.; Shreeve, Jean'ne M.
Journal of the American Chemical Society, 1981 , vol. 103, # 8 p. 1951 - 1952
反应条件
in autoclave, at 350°C, 5 h;
参考文献
Man et al.
Journal of the American Chemical Society, 1959 , vol. 81, p. 3575
反应条件
pyrolysis at 70°C, 1 h;
参考文献
Kitazume; Shreeve
Journal of the American Chemical Society, 1977 , vol. 99, p. 4194
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Kitazume, T.; Shreeve, J. M.
J. Inorg. Chem., 1978 , vol. 17, p. 2173 - 2176
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Gmelin Handbook: F: PerFHalOrg.SVol.3, 6.2.2, page 1 - 48
反应条件
Irradiation (UV/VIS); photolytic decomposition, 17 d;
参考文献
Gmelin Handbook: F: PerFHalOrg.2, 1.1.6.9, page 2 - 27
参考文献
Morse; Shreeve
Inorganic Chemistry, 1978 , vol. 17, p. 2169
参考文献
Morse; Shreeve
Inorganic Chemistry, 1978 , vol. 17, p. 2169
反应条件
anhyd. HCl, -78°C, 15 min;
参考文献
Kumar, Ramesh C.; Shreeve, Jean'ne M.
Journal of the American Chemical Society, 1981 , vol. 103, # 8 p. 1951 - 1952