water; NAF 1.) hexane, 0 grad C, Ar atmosphere, 1 h, 2.) methylenechloride, grad C, 0.5 h.; Yield given. Multistep reaction. Yields of byproduct given;

dihydrogen peroxide und Erwaermen des Reaktionsprodukts mit aethanol.Kalilauge auf 40grad;

T=180°C; unter Druck;

lead(IV) acetate; acetic acid

暂无反应条件数据

1.1: triethylamine / dichloromethane / 3 h / 25 °C / Inert atmosphere 2.1: potassium carbonate / methanol / 3 h / 25 °C 3.1: thiophene; n-butyllithium; copper (I) cyanide / tetrahydrofuran; hexane / 1 h / 25 °C / Inert atmosphere 3.2: 4 h / -78 - 25 °C / Inert atmosphere 4.1: tetrabutyl ammonium fluoride / tetrahydrofuran 5.1: 2,2,6,6-tetramethyl-1-piperidinyloxy, free radical; [bis(acetoxy)iodo]benzene / dichloromethane / 3 h / 25 °C View Scheme

silver carbonate in benzene 2 h; Heating;

tert.-butylhydroperoxide; potassium tert-butylate in water T=80°C; 8 h;

暂无反应条件数据

1: triethylamine / dichloromethane / 3 h / 25 °C / Inert atmosphere 2: potassium carbonate / methanol / 3 h / 25 °C View Scheme