3-苯基-吲哚-2-羧酸乙酯合成路线 （共 26 条）
反应条件
tetrakis(triphenylphosphine) palladium(0); sodium carbonate; lithium chloride in ethanol; toluene Condensation; 4 h; Heating;
参考文献
Bratton; Roth; Trivedi; Unangst
Journal of Heterocyclic Chemistry, 2000 , vol. 37, # 5 p. 1103 - 1108
反应条件
potassium carbonate; tetrakis(triphenylphosphine) palladium(0) in ethanol; water; toluene 48 h; Heating / reflux;
参考文献
CEPHALON FRANCE
Patent: EP1589016 A1, 2005 ;
Location in patent: Page/Page column 33-34 ;
反应条件
1: in benzene Heating; 2: With hydrogen; palladium on activated charcoal in benzene T=20°C;
参考文献
Penoni, Andrea; Volkmann, Jerome; Nicholas, Kenneth M.
Organic Letters, 2002 , vol. 4, # 5 p. 699 - 701
反应条件
1: With dirhodium tetraacetate in toluene T=80°C; 6 h; 2: With 1,8-diazabicyclo[5.4.0]undec-7-ene in toluene T=20°C; 2 h; Further stages.;
参考文献
Nakamura, Yoshinori; Ukita, Tatsuzo
Organic Letters, 2002 , vol. 4, # 14 p. 2317 - 2320
反应条件
carbon monoxide; 4 A molecular sieve; [(η5-C5Me5)Ru(CO)2]2 in 1,4-dioxane T=170°C; P=38787.1 Torr; 48 h; Title compound not separated from byproducts.;
参考文献
Penoni, Andrea; Nicholas, Kenneth M.
Chemical Communications, 2002 , # 5 p. 484 - 485
反应条件
thionyl chloride in ethanol T=80°C; Fischer indole synthesis; 0.666667 h;
参考文献
Yasui, Eiko; Wada, Masao; Takamura, Norio
Tetrahedron, 2009 , vol. 65, # 2 p. 461 - 468
反应条件
triphenylphosphine; cesium fluoride in toluene; acetonitrile T=50°C; 5.5 h;
参考文献
Hong, Deng; Chen, Zhengbo; Lin, Xufeng; Wang, Yanguang
Organic Letters, 2010 , vol. 12, # 20 p. 4608 - 4611
反应条件
thionyl chloride in ethanol T=80°C; Fischer indole synthesis; 0.666667 h;
参考文献
Yasui, Eiko; Wada, Masao; Takamura, Norio
Tetrahedron, 2009 , vol. 65, # 2 p. 461 - 468
反应条件
toluene-4-sulfonic acid in benzene T=80°C; Dehydration; deacetylation; 12 h;
参考文献
Collot, Valerie; Schmitt, Martine; Marwah, Padma; Bourguignon, Jean-Jacques
Heterocycles, 1999 , vol. 51, # 12 p. 2823 - 2847
反应条件
thionyl chloride in ethanol T=80°C; Fischer indole synthesis; 0.666667 h;
参考文献
Yasui, Eiko; Wada, Masao; Takamura, Norio
Tetrahedron, 2009 , vol. 65, # 2 p. 461 - 468
