S-甲基 N,N-二乙基硫代氨基甲酸酯合成路线 （共 18 条）
反应条件
sulfuryl dichloride T=0 - 20°C; 1 h;
参考文献
Mizuno, Takumi; Takahashi, Junko; Ogawa, Akiya
Tetrahedron, 2003 , vol. 59, # 8 p. 1327 - 1331
反应条件
3-chloro-benzenecarboperoxoic acid in chloroform T=0°C;
参考文献
Veverka, Karen A.; Johnson, Kenneth L.; Mays, Dennis C.; Lipsky, James J.; Naylor, Stephen
Biochemical Pharmacology, 1997 , vol. 53, # 4 p. 511 - 518
反应条件
in acetonitrile-H2 O; methanol hydrate
参考文献
Faiman; Morris D.
Patent: US5153219 A1, 1992 ;
反应条件
sodium periodate Oxidation;
参考文献
Mays, Dennis C.; Nelson, Albert N.; Fauq, Abdul H.; Shriver, Zachary H.; Veverka, Karen A.; et al.
Biochemical Pharmacology, 1995 , vol. 49, # 5 p. 693 - 700
反应条件
3-chloro-benzenecarboperoxoic acid in chloroform T=0°C; Oxidation;
参考文献
Mays, Dennis C.; Nelson, Albert N.; Fauq, Abdul H.; Shriver, Zachary H.; Veverka, Karen A.; et al.
Biochemical Pharmacology, 1995 , vol. 49, # 5 p. 693 - 700
反应条件
sodium periodate Oxidation;
参考文献
Mays, Dennis C.; Nelson, Albert N.; Fauq, Abdul H.; Shriver, Zachary H.; Veverka, Karen A.; et al.
Biochemical Pharmacology, 1995 , vol. 49, # 5 p. 693 - 700
反应条件
sulfur; selenium in tetrahydrofuran
T=30°C; 11 h; var. time, Se catalyst; Product distributionMechanism;
参考文献
Mizuno, Takumi; Nishiguchi, Ikuzo; Sonoda, Noboru
Tetrahedron, 1994 , vol. 50, # 19 p. 5669 - 5680
反应条件
sulfuric acid in chloroform
15 h; Heating;
参考文献
Tandel, Sagun K.; Rajappa, Srinivasachari; Pansare, Sunil V.
Tetrahedron, 1993 , vol. 49, # 34 p. 7479 - 7486
反应条件
in water
T=30 - 50°C;
参考文献
Degani, Iacopo; Fochi, Rita; Magistris, Claudio
Synthesis, 2009 , # 22 art. no. Z13109SS, p. 3807 - 3818
反应条件
1: carbon monoxide; diethylamine With selenium; sulfur in tetrahydrofuran
T=20°C; Carbonylation; substitution; P=760 Torr; 24 h;
2: methyl iodide in tetrahydrofuran
T=20°C; Esterification; 16 h; Title compound not separated from byproducts;
参考文献
Mizuno, Takumi; Kino, Takanobu; Takatoshi, Ito; Miyata, Toshiyuki
Synthetic Communications, 2000 , vol. 30, # 9 p. 1675 - 1688
