S-甲基 N,N-二乙基硫代氨基甲酸酯合成路线 （共 18 条）
反应条件
1: With triethylamine
T=50°C; neat (no solvent);
2: With dimethyl sulfate
T=60°C; 6 h; neat (no solvent);
参考文献
Degani, Iacopo; Fochi, Rita; Magistris, Claudio
Synthesis, 2009 , # 22 art. no. Z13109SS, p. 3807 - 3818
参考文献
Tilles
Journal of the American Chemical Society, 1959 , vol. 81, p. 714,716
反应条件
1: carbon oxide sulfide; diethylamine With sodium hydroxide
T=10°C; 4 h;
2: methyl iodide 2 h;
参考文献
Erve, John C. L.; Jensen, Ole N.; Valentine, Holly S.; Amarnath, Venkataraman; Valentine, William M.
Chemical Research in Toxicology, 2000 , vol. 13, # 4 p. 237 - 244
反应条件
in tetrahydrofuran
T=20°C; 2 h;
参考文献
Mizuno, Takumi; Takahashi, Junko; Ogawa, Akiya
Tetrahedron, 2003 , vol. 59, # 8 p. 1327 - 1331
参考文献
Degani, Iacopo; Fochi, Rita; Magistris, Claudio
Synthesis, 2009 , # 22 art. no. Z13109SS, p. 3807 - 3818
反应条件
2 h; Ambient temperature;
参考文献
Sonoda, Noboru; Mizuno, Takumi; Murakami, Sinkichi; Kondo, Kiyoshi; Ogawa, Akiya; at al.
Angewandte Chemie, 1989 , vol. 101, # 5 p. 476 - 477
反应条件
4 h; Ambient temperature;
参考文献
Mizuno, Takumi; Nishiguchi, Ikuzo; Sonoda, Noboru
Tetrahedron, 1994 , vol. 50, # 19 p. 5669 - 5680
反应条件
Yield given. Multistep reaction;
参考文献
Mizuno, Takumi; Nishiguchi, Ikuzo; Hirashima, Tsuneaki
Tetrahedron, 1993 , vol. 49, # 12 p. 2403 - 2412
