3,5-二甲基吡啶N-氧化物合成路线 (共 13 条)
反应条件
mercury(II) diacetate; bromine; acetic acid
T=70°C; 10 h; effect of metal ions; Product distributionMechanism;
参考文献
Klan, P.
Monatshefte fuer Chemie, 1993 , vol. 124, # 3 p. 327 - 330
反应条件
1.1: sulfuric acid; nitric acid / 6 h / 20 - 90 °C
2.1: palladium 10 on activated carbon / ethanol / 1 h / 90 °C / Inert atmosphere
2.2: 3 h / 90 °C / Inert atmosphere
View Scheme
参考文献
Fortage, Jerome; Peltier, Cyril; Perruchot, Christian; Takemoto, Yohei; Teki, Yoshio; Bedioui, Fethi; Marvaud, Valerie; Dupeyre, Gregory; Pospisil, Lubomir; Adamo, Carlo; Hromadova, Magdalena; Ciofini, Ilaria; Laine, Philippe P.
Journal of the American Chemical Society, 2012 , vol. 134, # 5 p. 2691 - 2705
反应条件
triethylamine in ethylene glycol dimethyl ether
1 h; Ambient temperature;
参考文献
Katagiri, Nobuya; Niwa, Ryuji; Furuya, Yoichi; Kato, Tetsuzo
Chemical and Pharmaceutical Bulletin, 1983 , vol. 31, # 6 p. 1833 - 1841