三氟-(三氟甲基硫基二硫基)甲烷合成路线 （共 61 条）
反应条件
sulfur in neat (no solvent)
reaction with an excess of sulfur in an autoclave at 200-280°C;;
参考文献
Emeleus, H. J.
Fortschr. Chem. Forsch., 1951 , vol. 2, p. 609 - 618
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Emeleus, H. J.
Suomen Kemistilehti B, 1958 , vol. 31, p. 101 - 109
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Gmelin Handbook: C: MVol.D2, 4.2.4.4.5, page 319 - 320
反应条件
sulfur(IV) fluoride; hydrogen fluoride; SCl2
T=80°C; 16 h; Yield given. Yields of byproduct given;
参考文献
Kunshenko, B. V.; Omarov, V. O.; Muratov, N. N.; Yagupol'skii, L. M.
Journal of Organic Chemistry USSR (English Translation), 1992 , vol. 28, # 5.1 p. 684 - 690
Zhurnal Organicheskoi Khimii, 1992 , vol. 28, # 5 p. 892 - 900
参考文献
Burg,A.B.; Parker,D.M.
Journal of the American Chemical Society, 1970 , vol. 92, p. 1898 - 1901
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Gmelin Handbook: F: PerFHalOrg.3, 1.1.2, page 9 - 14
反应条件
sulfur(IV) fluoride; hydrogen fluoride; chlorine
T=80°C; 10 h; Yield given. Yields of byproduct given;
参考文献
Kunshenko, B. V.; Omarov, V. O.; Muratov, N. N.; Yagupol'skii, L. M.
Journal of Organic Chemistry USSR (English Translation), 1992 , vol. 28, # 5.1 p. 684 - 690
Zhurnal Organicheskoi Khimii, 1992 , vol. 28, # 5 p. 892 - 900
反应条件
SCl2 in xylene
0.75 h; Ambient temperature; Yield given. Title compound not separated from byproducts;
参考文献
Munavalli, Shekar; Rossman, David I.; Rohrbaugh, Dennis K.; Ferguson, C. Parker; Szafraniec, Leonard J.
Journal of Fluorine Chemistry, 1992 , vol. 59, # 1 p. 91 - 99
参考文献
Gombler, W.
Zeitschrift fuer Anorganische und Allgemeine Chemie, 1975 , vol. 416, p. 235 - 239
反应条件
potassium fluoride
with active KF;
参考文献
Gombler, W.
Zeitschrift fuer Anorganische und Allgemeine Chemie, 1975 , vol. 416, p. 235 - 239
反应条件
in acetonitrile
T=80 - 90°C; 4 h;
参考文献
Munavalli; Rossman; Rohrbaugh; Ferguson; Durst
Journal of Fluorine Chemistry, 1996 , vol. 76, # 1 p. 7 - 13
反应条件
T=85 - 95°C; 6 h; Further byproducts given;
参考文献
Munavalli, S.; Rossman, D. I.; Rohrbaugh, D. K.; Ferguson, C. P.; Buettner, L.
Journal of Fluorine Chemistry, 1993 , vol. 65, # 1-2 p. 15 - 20
参考文献
Zack; Shreeeve
Inorganic and Nuclear Chemistry Letters, 1974 , vol. 10, p. 619
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Zack, N. R.; Shreeve, J. M.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry, 1975 , p. 614 - 616
