双(三氟甲基)二硫化物合成路线 (共 250 条)
反应条件
pentacarbonyliron(0) in tetrahydrofuran T=-80°C;
参考文献
Harris,J.F.
Journal of the American Chemical Society, 1962 , vol. 84, p. 3148 - 3153
反应条件
triethylamine in dichloromethane T=10°C; 0.166667 h;
参考文献
Lopusinski, Andrezej
Phosphorus, Sulfur and Silicon and the Related Elements, 1990 , vol. 47, p. 383 - 390
反应条件
trimethylsilylazide; hexachlorocyclo-1,3-pentadiene in toluene T=110°C; P=0.01 Torr; 3 h;
参考文献
Haas, Alois; Mischo, Thomas
Canadian Journal of Chemistry, 1989 , vol. 67, p. 1902 - 1908
反应条件
hydrogen bromide in further solvent(s) 160-175°C; solvent: tetramethylenesulfone;
参考文献
Gmelin Handbook: F: PerFHalOrg.1, 1.1.6.6, page 195 - 217
反应条件
potassium fluoride; carbonic difluoride in acetonitrile
参考文献
Ratcliffe,C.T.; Shreeve,J.M.
Journal of the American Chemical Society, 1968 , vol. 90, p. 5403 - 5408
反应条件
silver(II) fluoride; NAF in 1,2,2-trifluoro-trichloroethane
参考文献
Sheppard,W.A.
Journal of the American Chemical Society, 1962 , vol. 84, p. 3058 - 3063
反应条件
trimethylsilylazide in monofluoro-trichloromethane T=-30°C; 24 h;
参考文献
Bielefeldt, Dietmar; Haas, Alois
Chemische Berichte, 1983 , vol. 116, # 3 p. 1257 - 1260
反应条件
in monofluoro-trichloromethane T=-73.1°C; 6 h; Irradiation;
参考文献
Schlosser, K.; Steenken, S.
Journal of the American Chemical Society, 1983 , vol. 105, # 6 p. 1504 - 1506
反应条件
thionyl chloride in tetrachloromethane byproducts: SO2;
参考文献
Gmelin Handbook: F: PerFHalOrg.2, 1.1.6.11, page 32 - 49
反应条件
nitrosyl chloride in neat (no solvent) below ambient temp.;;
参考文献
Gmelin Handbook: Cl: SVol.B2, 93, page 517 - 519