双(三氟甲基)二硫化物合成路线 (共 250 条)
反应条件
390-420°C, atm. pessure in a continuous flow system;
参考文献
Gmelin Handbook: F: PerFHalOrg.SVol.2, 6.2.1.6.5, page 172 - 209
反应条件
in diethyl ether -78°C, among other products;
参考文献
Gmelin Handbook: F: PerFHalOrg.SVol.2, 6.2.1.6.5, page 172 - 209
反应条件
in diethyl ether -78°C;
参考文献
Gmelin Handbook: F: PerFHalOrg.SVol.2, 6.2.1.6.5, page 172 - 209
反应条件
dichloro-trifluoromethyl-λ3-iodane in N,N-dimethyl-formamide; acetonitrile T=-78°C; 18 h; Title compound not separated from byproducts;
参考文献
Tyrra, Wieland; Naumann, Dieter
Journal of Fluorine Chemistry, 1989 , vol. 45, p. 401 - 416
反应条件
buta-1,3-diene in toluene T=110°C; 3 h;
参考文献
Haas, Alois; Mischo, Thomas
Canadian Journal of Chemistry, 1989 , vol. 67, p. 1902 - 1908
反应条件
2,2'-azo-bisisobutyronitrile in benzene byproducts: HCl; Irradiation (UV/VIS);
参考文献
Gmelin Handbook: F: PerFHalOrg.1, 1.1.6.5.2, page 157 - 193
反应条件
in further solvent(s) 150-160°C; solvent: tetramethylenesulfone;
参考文献
Gmelin Handbook: F: PerFHalOrg.1, 1.1.6.6, page 195 - 217
参考文献
Gmelin Handbook: F: PerFHalOrg.1, 1.1.6.6, page 195 - 217
反应条件
sulfur(IV) fluoride T=250°C;
参考文献
Middleton,W.J. et al.
Journal of Organic Chemistry, 1965 , vol. 30, p. 1375 - 1384
反应条件
in toluene T=110°C; P=0.01 Torr; 3 h;
参考文献
Haas, Alois; Mischo, Thomas
Canadian Journal of Chemistry, 1989 , vol. 67, p. 1902 - 1908