双(三氟甲基)二硫化物合成路线 （共 250 条）
反应条件
sulfur in neat (no solvent) byproducts: polysulfane; reaction in an autoclave at 265°C for 24 hours;;
参考文献
Brand, G. A. R.; Emeleus, H. J.; Haszeldine, R. N.
Journal of the Chemical Society, 1952 , p. 2198 - 2205
Full Text Show Details
Gmelin Handbook: C: MVol.D2, 4.2.4.4.5, page 319 - 320
反应条件
sulfur(IV) fluoride; hydrogen fluoride; chlorine T=80°C; 10 h; Yield given. Yields of byproduct given;
参考文献
Kunshenko, B. V.; Omarov, V. O.; Muratov, N. N.; Yagupol'skii, L. M.
Journal of Organic Chemistry USSR (English Translation), 1992 , vol. 28, # 5.1 p. 684 - 690
Zhurnal Organicheskoi Khimii, 1992 , vol. 28, # 5 p. 892 - 900
参考文献
Haas,A.; Lieb,M.; Zhang,Y.
Journal of Fluorine Chemistry, 1985 , vol. 29, p. 297
参考文献
Munavalli, S.; Rossman, D. I.; Rohrbaugh, D. K.; Ferguson, C. P.; Buettner, L.
Journal of Fluorine Chemistry, 1993 , vol. 65, # 1-2 p. 15 - 20
反应条件
SCl2 in xylene 0.75 h; Ambient temperature; Yield given. Title compound not separated from byproducts;
参考文献
Munavalli, Shekar; Rossman, David I.; Rohrbaugh, Dennis K.; Ferguson, C. Parker; Szafraniec, Leonard J.
Journal of Fluorine Chemistry, 1992 , vol. 59, # 1 p. 91 - 99
反应条件
Copper(I) trifluoromethanethiolate T=80 - 90°C; 4 h; Further byproducts given. Title compound not separated from byproducts;
参考文献
Munavalli; Rossman; Rohrbaugh; Ferguson; Durst
Journal of Fluorine Chemistry, 1996 , vol. 76, # 1 p. 7 - 13
参考文献
Gmelin Handbook: F: PerFHalOrg.2, 1.2, page 50 - 76
反应条件
in acetonitrile byproducts: SO2;
参考文献
Gmelin Handbook: F: PerFHalOrg.2, 1.1.6.11, page 32 - 49
参考文献
Gmelin Handbook: F: PerFHalOrg.SVol.2, 6.2.1.6.5, page 172 - 209
反应条件
in acetonitrile T=80 - 90°C; 4 h;
参考文献
Munavalli; Rossman; Rohrbaugh; Ferguson; Durst
Journal of Fluorine Chemistry, 1996 , vol. 76, # 1 p. 7 - 13
