双(三氟甲基)二硫化物合成路线 （共 250 条）
反应条件
in pentane T=-78 - 20°C; Title compound not separated from byproducts;
参考文献
Munavalli; Rohrbaugh; Rossman; Berg; Durst
Phosphorus, Sulfur and Silicon and the Related Elements, 2004 , vol. 179, # 8 p. 1645 - 1655
反应条件
180°C; chrom oxide fluoride catalyst;
参考文献
Gmelin Handbook: F: PerFHalOrg.1, 1.1.6.5.2, page 157 - 193
参考文献
Gmelin Handbook: F: PerFHalOrg.1, 1.1.6.5.2, page 157 - 193
反应条件
Irradiation (UV/VIS); educts used in 1:1 ratio; isomers not possible to separate;
参考文献
Gmelin Handbook: F: PerFHalOrg.2, 1.1.6.9, page 2 - 27
参考文献
Middleton,W.J. et al.
Journal of Organic Chemistry, 1965 , vol. 30, p. 1375 - 1384
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Gmelin Handbook: F: PerFHalOrg.1, 1.1.5.1, page 48 - 56
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E. I. Du Pont de Nemours & Co.
Patent: GB857651 , 1961 ;
C.A., 1961 , p. 11919
Full Text Show Details
E. I. Du Pont de Nemours & Co.
Patent: US3117977 , 1964 ;
C.A., 1964 , vol. 60, p. 6849
反应条件
in tetrachloromethane room temp.;
参考文献
Gmelin Handbook: F: PerFHalOrg.2, 1.1.6.11, page 32 - 49
参考文献
Gmelin Handbook: F: PerFHalOrg.1, 1.1.6.5.3, page 193 - 194
反应条件
T=85 - 95°C; 6 h; Further byproducts given;
参考文献
Munavalli, S.; Rossman, D. I.; Rohrbaugh, D. K.; Ferguson, C. P.; Buettner, L.
Journal of Fluorine Chemistry, 1993 , vol. 65, # 1-2 p. 15 - 20
反应条件
T=45°C; 12 h; Yield given;
参考文献
Henn, R.; Sundermeyer, W.; Witz, M.; Pritzkow, H.
Journal of Fluorine Chemistry, 1989 , vol. 45, p. 225 - 238
反应条件
in neat (no solvent) -20°C;
参考文献
Gmelin Handbook: F: PerFHalOrg.1, 1.1.6.5.2, page 157 - 193
