双(三氟甲基)二硫化物合成路线 （共 250 条）
反应条件
CF3SH:S2O6F2 molar ratio 1:1, from -183 to +25°C;
参考文献
Kirchmeier; Shreeve
Inorganic Chemistry, 1973 , vol. 12, p. 2886,2888, 2889, 2890
反应条件
water byproducts: HCl, COS; HCl excess; 20°C for 3 h; 9 h shaking;
参考文献
Gmelin Handbook: F: PerFHalOrg.1, 1.1.6.5.2, page 157 - 193
反应条件
water byproducts: HCl; shaking for 12-24 h; first less H2O, later H2O excess;
参考文献
Gmelin Handbook: F: PerFHalOrg.1, 1.1.6.5.2, page 157 - 193
反应条件
sodium hydroxide byproducts: NaCl, H2O;
参考文献
Gmelin Handbook: F: PerFHalOrg.1, 1.1.6.5.2, page 157 - 193
反应条件
in tetrachloromethane 0 or 20°C;
参考文献
Gmelin Handbook: F: PerFHalOrg.2, 1.1.6.11, page 32 - 49
反应条件
in liquid sulphur dioxide -78°C;
参考文献
Gmelin Handbook: F: PerFHalOrg.SVol.2, 6.2.1.6.5, page 172 - 209
反应条件
byproducts: CF3SH, S, KF*HF; warming to 25°C in the presence of excess KF;
参考文献
Burton,C.A.; Shreeve,J.M.
Journal of the American Chemical Society, 1976 , vol. 98, p. 6545 - 6547
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Gmelin Handbook: F: PerFHalOrg.SVol.2, 6.2.1.6.5, page 172 - 209
反应条件
byproducts: CF3SH, S, CsF*HF; warming to 25°C in the presence of excess CsF;
参考文献
Burton,C.A.; Shreeve,J.M.
Journal of the American Chemical Society, 1976 , vol. 98, p. 6545 - 6547
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Gmelin Handbook: F: PerFHalOrg.SVol.2, 6.2.1.6.5, page 172 - 209
反应条件
pyridine T=20°C; 12 h; other sulfenyl chloride;
参考文献
Gerstenberger, M. R. C.; Haas, A.
Journal of Fluorine Chemistry, 1983 , vol. 23, p. 525 - 540
反应条件
T=500°C; unter Druck;
参考文献
Dannley; Taborsky
Journal of Organic Chemistry, 1957 , vol. 22, p. 1275
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Man et al.
Journal of the American Chemical Society, 1959 , vol. 81, p. 3575
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Du Pont de Nemours and Co.
Patent: US2729663 , 1954 ;
