咪唑并[2,1-f]吡啶-5-甲醛合成路线 (共 3 条)
反应条件
manganese(IV) oxide in chloroform
1.5 h; Heating;
参考文献
Chezal; Moreau; Delmas; Gueiffier; Blache; Grassy; Lartigue; Chavignon; Teulade
Journal of Organic Chemistry, 2001 , vol. 66, # 20 p. 6576 - 6584
反应条件
diisobutylaluminium hydride in dichloromethane
T=-70°C; 3 h;
参考文献
Chezal; Moreau; Delmas; Gueiffier; Blache; Grassy; Lartigue; Chavignon; Teulade
Journal of Organic Chemistry, 2001 , vol. 66, # 20 p. 6576 - 6584
反应条件
1: 80 percent / NaHCO3 / aq. ethanol / 9 h / Heating
2: 79 percent / DIBAL-H / CH2Cl2 / 3 h / -70 °C
View Scheme
参考文献
Moreau, Emmanuel; Chezal, Jean-Michel; Dechambre, Caroline; Canitrot, Damien; Blache, Yves; Lartigue, Claire; Chavignon, Olivier; Teulade, Jean-Claude
Heterocycles, 2002 , vol. 57, # 1 p. 21 - 38