3-羟基-7,8,9,10-四氢苯并[c]苯并吡喃-6-酮合成路线 （共 18 条）
反应条件
1: aqueous sulfuric acid
2: Erhitzen auf Temperaturen oberhalb des Schmelzpunkts
View Scheme
参考文献
Desai et al.
Proceedings - Indian Academy of Sciences, Section A, 1947 , # 25 p. 345,347
反应条件
1: phosphoryl chloride
2: alkaline solution
3: Erhitzen auf Temperaturen oberhalb des Schmelzpunkts
View Scheme
参考文献
Desai et al.
Proceedings - Indian Academy of Sciences, Section A, 1947 , # 25 p. 345,347
反应条件
sulfuric acid
Kochen des Reaktionsprodukts mit Kalilauge;
参考文献
Sen; Basu
Journal of the Indian Chemical Society, 1928 , vol. 5, p. 473
Chem. Zentralbl., 1928 , vol. 99, # II p. 2241
反应条件
Erhitzen auf Temperaturen oberhalb des Schmelzpunkts;
参考文献
Desai et al.
Proceedings - Indian Academy of Sciences, Section A, 1947 , # 25 p. 345,347
参考文献
Pisani, Leonardo; Catto, Marco; Giangreco, Ilenia; Leonetti, Francesco; Nicolotti, Orazio; Stefanachi, Angela; Cellamare, Saverio; Carotti, Angelo
ChemMedChem, 2010 , vol. 5, # 9 p. 1616 - 1630
反应条件
1: potassium carbonate / N,N-dimethyl-formamide / 24 h / 20 °C
2: 2,3-dicyano-5,6-dichloro-p-benzoquinone / 1,4-dioxane / 24 h / Reflux
View Scheme
参考文献
Pisani, Leonardo; Catto, Marco; Giangreco, Ilenia; Leonetti, Francesco; Nicolotti, Orazio; Stefanachi, Angela; Cellamare, Saverio; Carotti, Angelo
ChemMedChem, 2010 , vol. 5, # 9 p. 1616 - 1630
反应条件
potassium carbonate; acetone
参考文献
Losco; Peri
Gazzetta Chimica Italiana, 1959 , vol. 89, p. 1298,1304
反应条件
T=190 - 200°C; beim Schmelzen;
参考文献
Sen; Basu
Journal of the Indian Chemical Society, 1928 , vol. 5, p. 473
Chem. Zentralbl., 1928 , vol. 99, # II p. 2241
