3-甲氧基氧杂蒽-9-酮合成路线 （共 39 条）
反应条件
1: glacial acetic acid; concentrated sulfuric acid
2: sulfuric acid / Diazotization
View Scheme
参考文献
Ullmann; Denzler
Chemische Berichte, 1906 , vol. 39, p. 4337
反应条件
1: NaOH-solution
2: potassium permanganate; water
3: KOH; copper powder; alcohol / 200 °C
4: concentrated sulfuric acid / 100 °C
View Scheme
参考文献
Ullmann; Wagner
Justus Liebigs Annalen der Chemie, 1907 , vol. 355, p. 366
Justus Liebigs Annalen der Chemie, 1909 , vol. 371, p. 388
反应条件
1: KOH; copper powder; alcohol / 200 °C
2: concentrated sulfuric acid / 100 °C
View Scheme
参考文献
Ullmann; Wagner
Justus Liebigs Annalen der Chemie, 1907 , vol. 355, p. 366
Justus Liebigs Annalen der Chemie, 1909 , vol. 371, p. 388
反应条件
1: potassium permanganate; water
2: KOH; copper powder; alcohol / 200 °C
3: concentrated sulfuric acid / 100 °C
View Scheme
参考文献
Ullmann; Wagner
Justus Liebigs Annalen der Chemie, 1907 , vol. 355, p. 366
Justus Liebigs Annalen der Chemie, 1909 , vol. 371, p. 388
反应条件
1: Reaktion ueber mehrere Stufen
2: NaOH-solution
3: potassium permanganate; water
4: KOH; copper powder; alcohol / 200 °C
5: concentrated sulfuric acid / 100 °C
View Scheme
参考文献
Ullmann; Wagner
Justus Liebigs Annalen der Chemie, 1907 , vol. 355, p. 366
Justus Liebigs Annalen der Chemie, 1909 , vol. 371, p. 388
反应条件
1: ethanolic sodium ethylate; copper-powder
2: tin (IV)-chloride / 130 °C
View Scheme
参考文献
Neunhoeffer; Haase
Chemische Berichte, 1958 , vol. 91, p. 1801,1804
反应条件
carbon disulfide; aluminium trichloride
参考文献
Asahina; Tanase
Proceedings of the Imperial Academy (Tokyo), 1940 , vol. 16, p. 297
Yakugaku Zasshi, 1941 , vol. 61, p. 129,131
参考文献
Goldberg; Wragg
Journal of the Chemical Society, 1958 , p. 4227,4230
反应条件
1: 100 percent / pyridine*HCl / 2 h / 180 - 200 °C
2: 95 percent / K2CO3 / dimethylformamide / 1 h / 55 - 65 °C
3: 68 percent / various solvent(s) / 4 h / 185 - 195 °C
View Scheme
参考文献
Sato; Dan; Onuma; Tanaka; Koga
Chemical and Pharmaceutical Bulletin, 1990 , vol. 38, # 5 p. 1266 - 1277
