反应条件
1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; 4-(N,N-dimethlyamino)pyridine / dichloromethane / 20 °C
2: palladium diacetate; 1,1'-bis-(diphenylphosphino)ferrocene; cesium fluoride / acetonitrile; toluene / 18 h / 80 °C / |Glovebox; |Sealed tube
View Scheme
参考文献
Dong, Ying; Liu, Bangyu; Chen, Peng; Liu, Qun; Wang, Mang
Angewandte Chemie - International Edition, 2014 , vol. 53, # 13 p. 3442 - 3446
Angew. Chem., 2014 , vol. 126, # 13 p. 3510 - 3514,5