1: 0.19 g / conc. H2SO4 / 6 h / Heating
2: 0.14 g / LiAlH4 / tetrahydrofuran / 24 h / Ambient temperature
3: 0.1 g / pyridine / 25 h / Ambient temperature
View Scheme
参考文献
Majee, R. N.; Ramani, R.
Journal of the Indian Chemical Society, 1993 , vol. 70, # 2 p. 167 - 168
1: oleic acid; 18:2 ω-6; palmitoleic acid; ethyl stearic acid; hexadecanoic acid; octadecanoic acid With Grubbs II
T=50 - 53°C; 20 - 72 h; Neat (no solvent);
2: With ethyl vinyl ether
3: methanol With sulfuric acid
Product distribution / selectivity;
参考文献
The United States of America as represented by the Secretary of Agriculture
Patent: US7534917 B1, 2009 ;
Location in patent: Page/Page column 12-13; 18 ;
1: oleic acid; 18:2 ω-6; palmitoleic acid; ethyl stearic acid; hexadecanoic acid; octadecanoic acid; 18:3 ω-3 With Grubbs II
T=50 - 75°C; 8 - 72 h; Neat (no solvent);
2: With ethyl vinyl ether
3: methanol With sulfuric acid
1 h; Heating / reflux; Product distribution / selectivity;
参考文献
The United States of America as represented by the Secretary of Agriculture
Patent: US7534917 B1, 2009 ;
Location in patent: Page/Page column Sheet 5/6; 11; 12; 14; 18 ;
