乙基2-二乙氧基磷酰-3-氧代丁酸酯合成路线 （共 7 条）
反应条件
water 2.5 h; Heating; Yield given;
参考文献
Amarnath, Venkataraman; Amarnath, Kalyani; Masterson, Tina; Davies, Sean; Roberts II, Jackson
Synthetic Communications, 2005 , vol. 35, # 3 p. 397 - 408
反应条件
1: ethyl acetoacetate With sodium in diethyl ether
2: diethyl chlorophosphinate in diethyl ether
T=20°C; 2 h;
参考文献
Vizer; Erzhanov; Manchuk
Russian Journal of Organic Chemistry, 2000 , vol. 36, # 7 p. 1072 - 1074
反应条件
triethylamine; magnesium chloride
1) CH2Cl2, room temperature, 30 min, 2) 20 deg C; Multistep reaction;
参考文献
Corbel, Bernard; L'Hostis-Kervella, Isabelle; Haelters, Jean-Pierre
Synthetic Communications, 1996 , vol. 26, # 13 p. 2561 - 2568
反应条件
triethylamine; magnesium chloride
1) CH2Cl2, room temperature, 30 min, 2) 20 deg C; Multistep reaction;
参考文献
Corbel, Bernard; L'Hostis-Kervella, Isabelle; Haelters, Jean-Pierre
Synthetic Communications, 1996 , vol. 26, # 13 p. 2561 - 2568
参考文献
Kreutzkamp
Chemische Berichte, 1955 , vol. 88, p. 195,198
Full Text Show Details
Kirilov; Petrov
Monatshefte fuer Chemie, 103<1972,1651,1656
参考文献
Kirilov,M.; Petrov,G.
Monatshefte fuer Chemie, 1972 , vol. 103, p. 1651 - 1660
参考文献
Arbusow et al.
Zhurnal Obshchei Khimii, 1950 , vol. 20, p. 1468,1475; engl. Ausg. S. 1529, 1536
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1959 , p. 41,46; engl. Ausg. S. 37, 41
Full Text Show Details
Kreutzkamp; Kayser
Justus Liebigs Annalen der Chemie, 1957 , vol. 609, p. 39,45
