3,3,4,4,4-五氟丁烷-2-酮合成路线 （共 16 条）
反应条件
water; triethylamine in acetonitrile T=45 - 60°C; 5 h;
参考文献
Cheburkov, Yuri; Moore, George G.I.
Journal of Fluorine Chemistry, 2003 , vol. 123, # 2 p. 227 - 231
反应条件
sulfuric acid; water; acetic acid Reagens 4: Natriumdichromat;
参考文献
McBee et al.
Journal of the American Chemical Society, 1952 , vol. 74, p. 1387,1390
反应条件
methyl-magnesium iodide
参考文献
Dishart; Levine
Journal of the American Chemical Society, 1956 , vol. 78, p. 2268
反应条件
tris(2-methoxyethyl)amine; water in N,N-dimethyl-formamide
参考文献
Sud'enkov,Yu.Ya.
Journal of Organic Chemistry USSR (English Translation), 1978 , vol. 14, p. 1240 - 1241
Zhurnal Organicheskoi Khimii, 1978 , vol. 14, # 6 p. 1336 - 1337
反应条件
1: With triethylamine; tert-butyl alcohol T=55 - 60°C; 20 h; 2: With toluene-4-sulfonic acid T=110 - 115°C; 3 h; 3: With water; triethylamine Heating; Title compound not separated from byproducts;
参考文献
Cheburkov, Yuri; Moore, George G.I.
Journal of Fluorine Chemistry, 2003 , vol. 123, # 2 p. 227 - 231
反应条件
1: With triethylamine; tert-butyl alcohol T=55 - 60°C; 20 h; 2: With toluene-4-sulfonic acid T=115°C; 3 h; 3: With water; triethylamine Heating; Title compound not separated from byproducts;
参考文献
Cheburkov, Yuri; Moore, George G.I.
Journal of Fluorine Chemistry, 2003 , vol. 123, # 2 p. 227 - 231
反应条件
in anhydrous butyl ether
参考文献
Moore,R.A.; Levine,R.
Journal of Organic Chemistry, 1964 , vol. 29, p. 1439 - 1444
反应条件
sulfuric acid; mercuric sulphate
参考文献
Haszeldine; Leedham
Journal of the Chemical Society, 1952 , p. 3483,3489
参考文献
Haszeldine; Leedham
Journal of the Chemical Society, 1952 , p. 3483,3489
参考文献
McBee et al.
Journal of the American Chemical Society, 1952 , vol. 74, p. 1387,1390
