反应条件
1.1: 99 percent / LiAlH4 / diethyl ether / 1.5 h / 0 °C
2.1: TPAP; NMO; 4 Angstroem molecular sieves / CH2Cl2 / 0.17 h / 20 °C
3.1: K2CO3 / methanol / 1 h / 20 °C
4.1: 95 percent / BCl3*SMe2 / CH2Cl2 / 0.25 h / 20 °C
5.1: 96 percent / nBu3P / tetrahydrofuran / 3 h / 20 °C
6.1: silica gel / 72 h / 20 °C
6.2: 66 percent / aq. ammonium cerium nitrate / diethyl ether / 1 h / 20 °C
7.1: 80 percent / OsO4; pyridine / 24 h
8.1: 95 percent / H2O2 / tetrahydrofuran / 16 h
9.1: 4 Angstroem molecular sieves
10.1: NaH; pyridine / 1 h / 20 °C
View Scheme
