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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
3742-78-7
合成路线
（共 6 条）
1332864-87-5
→
反应条件
3742-78-7
反应条件
1.1: ethylenediamine / tetrahydrofuran / 0 - 20 °C / Inert atmosphere 2.1: iodosylbenzene / tetrahydrofuran / 20 °C / Inert atmosphere 3.1: acetic acid; zinc / tetrahydrofuran / 0 - 20 °C / Inert atmosphere 4.1: hydrogenchloride / dioxanes / 24 h / Inert atmosphere 4.2: 48 h 4.3: Inert atmosphere View Scheme
参考文献
Strick, Benjamin F.; Mundal, Devon A.; Thomson, Regan J.
Journal of the American Chemical Society, 2011 , vol. 133, # 36 p. 14252 - 14255
1332864-88-6
→
反应条件
3742-78-7
反应条件
1.1: iodosylbenzene / tetrahydrofuran / 20 °C / Inert atmosphere 2.1: acetic acid; zinc / tetrahydrofuran / 0 - 20 °C / Inert atmosphere 3.1: hydrogenchloride / dioxanes / 24 h / Inert atmosphere 3.2: 48 h 3.3: Inert atmosphere View Scheme
参考文献
Strick, Benjamin F.; Mundal, Devon A.; Thomson, Regan J.
Journal of the American Chemical Society, 2011 , vol. 133, # 36 p. 14252 - 14255
1332864-97-7
→
反应条件
3742-78-7
反应条件
1.1: acetic acid; zinc / tetrahydrofuran / 0 - 20 °C / Inert atmosphere 2.1: hydrogenchloride / dioxanes / 24 h / Inert atmosphere 2.2: 48 h 2.3: Inert atmosphere View Scheme
参考文献
Strick, Benjamin F.; Mundal, Devon A.; Thomson, Regan J.
Journal of the American Chemical Society, 2011 , vol. 133, # 36 p. 14252 - 14255
932-89-8
2-环己基亚基-乙醇
→
反应条件
3742-78-7
反应条件
1.1: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran / 0 - 20 °C / Inert atmosphere 2.1: ethylenediamine / tetrahydrofuran / 0 - 20 °C / Inert atmosphere 3.1: iodosylbenzene / tetrahydrofuran / 20 °C / Inert atmosphere 4.1: acetic acid; zinc / tetrahydrofuran / 0 - 20 °C / Inert atmosphere 5.1: hydrogenchloride / dioxanes / 24 h / Inert atmosphere 5.2: 48 h 5.3: Inert atmosphere View Scheme
参考文献
Strick, Benjamin F.; Mundal, Devon A.; Thomson, Regan J.
Journal of the American Chemical Society, 2011 , vol. 133, # 36 p. 14252 - 14255
1332865-16-3
+
75-36-5
乙酰氯
→
反应条件
3742-78-7
反应条件
1: tert-butyl 2-(1-vinylcyclohexyl)hydrazinecarboxylate With hydrogenchloride in dioxanes 24 h; Inert atmosphere; 2: With platinum(IV) oxide; hydrogen in methanol 48 h; 3: acetyl chloride With 4-(N,N-dimethlyamino)pyridine; triethylamine Inert atmosphere;
参考文献
Strick, Benjamin F.; Mundal, Devon A.; Thomson, Regan J.
Journal of the American Chemical Society, 2011 , vol. 133, # 36 p. 14252 - 14255
1940-18-7
1-乙基环己醇
+
75-05-8
乙腈
→
反应条件
3742-78-7
反应条件
ammonium cerium(IV) nitrate
参考文献
Nikishin,G.I. et al.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1977 , vol. 26, p. 1420 - 1424
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1977 , vol. 26, p. 1548 - 1552
