(E)-3-碘-2-丁烯-1-醇合成路线 （共 7 条）
反应条件
pyridine; 4-(N,N-dimethlyamino)pyridine in dichloromethane 16 h; Ambient temperature; Yield given;
参考文献
Borhan, Babak; Souto, Maria L.; Um, Joann M.; Zhou, Bishan; Nakanishi, Koji
Chemistry - A European Journal, 1999 , vol. 5, # 4 p. 1172 - 1175
反应条件
copper(l) iodide; triethylamine; tetrakis(triphenylphosphine) palladium(0) in tetrahydrofuran T=20°C; Sonogashira reaction; 2 h;
参考文献
Murakami, Yusuke; Nakano, Masayuki; Shimofusa, Takuya; Furuichi, Noriyuki; Katsumura, Shigeo
Organic and Biomolecular Chemistry, 2005 , vol. 3, # 8 p. 1372 - 1374
反应条件
1: With bis(cyclopentadienyl)titanium dichloride; chloro-(2-methylpropyl)magnesium in diethyl ether
T=0 - 20°C; 4 h; Inert atmosphere;
2: With iodine in diethyl ether
T=-78 - 0°C; 1 h; Inert atmosphere;
参考文献
Paterson, Ian; Anderson, Edward A.; Dalby, Stephen M.; Lim, Jong Ho; Maltas, Philip; Loiseleur, Olivier; Genovino, Julien; Moessner, Christian
Organic and Biomolecular Chemistry, 2012 , vol. 10, # 30 p. 5861 - 5872
反应条件
iodine; sodium carbonate in dichloromethane
T=0°C; 0.166667 h;
参考文献
Murakami, Yusuke; Nakano, Masayuki; Shimofusa, Takuya; Furuichi, Noriyuki; Katsumura, Shigeo
Organic and Biomolecular Chemistry, 2005 , vol. 3, # 8 p. 1372 - 1374
反应条件
diisobutylaluminium hydride in hexane; toluene
T=0°C; 0.5 h;
参考文献
Chen, Sui-Hui; Horvath, Raymond F.; Joglar, Jesus; Fisher, Matthew J.; Danishefsky, Samuel J.
Journal of Organic Chemistry, 1991 , vol. 56, # 20 p. 5834 - 5845
反应条件
lithium aluminium tetrahydride; aluminium trichloride in diethyl ether
T=0°C; 1 h;
参考文献
Ooi, Takashi; Hokke, Yasutoshi; Tayama, Eiji; Maruoka, Keiji
Tetrahedron, 2001 , vol. 57, # 1 p. 135 - 144
参考文献
Nesnas, Nasri; Rando, Robert R; Nakanishi, Koji
Tetrahedron, 2002 , vol. 58, # 32 p. 6577 - 6584
