5-氨基-2,4,6-三碘异酞酰氯合成路线 (共 14 条)
反应条件
pyridine; thionyl chloride in 1,2-dichloro-ethane T=70 - 85°C; 8.5 h;
参考文献
GE HEALTHCARE AS
Patent: WO2008/123779 A1, 2008 ;
Location in patent: Page/Page column 12; 14; 15 ;
参考文献
Mitsui Toatsu Chemicals, Inc.
Patent: US5750779 A1, 1998 ;
参考文献
Mitsui Toatsu Chemicals, Inc.
Patent: US5750779 A1, 1998 ;
反应条件
1: 73 percent / ICl; KCl / H2O / 24 h / 55 °C 2: 89.3 percent / SOCl2 / 6 h / Heating View Scheme
参考文献
Pillai, K. M. R.; Diamantidis, G.; Duncan, L.; Ranganathan, R. S.
Journal of Organic Chemistry, 1994 , vol. 59, # 6 p. 1344 - 1350
反应条件
thionyl chloride in acetic acid
参考文献
Dibra S.p.A.
Patent: US5965772 A1, 1999 ;
参考文献
Guerbet S.A.
Patent: US4107286 A1, 1978 ;
反应条件
sulfuric acid in acetonitrile Product distribution / selectivity;
参考文献
MANAC INC.
Patent: WO2006/100731 A1, 2006 ;
Location in patent: Page/Page column 6 ;
反应条件
lithium hydroxide; dimethylammonium 2,4-dichlorophenoxyacetate in ethanol; water; ethyl acetate; acetyl chloride
参考文献
Abbott Laboratories
Patent: US5705692 A1, 1998 ;
参考文献
Mallinckrodt, Inc.
Patent: US5075502 A1, 1991 ;
参考文献
Bracco Industria Chimica S.p.A.
Patent: US4139605 A1, 1979 ;