二甲基2-(苯基甲氧羰基氨基)丙二酸酯合成路线 （共 6 条）
反应条件
1: 100 percent / K2CO3, 18-crown-6 / dimethylformamide / 1 h / 100 - 110 °C 2: 91 percent / aq. NaOH / Heating View Scheme
参考文献
Polish Journal of Chemistry, , vol. 54, # 6 p. 1327 - 1329
反应条件
pyridine in dichloromethane
T=0°C; 0.0833333 h;
参考文献
Yamada, Ken; Kurokawa, Toshiki; Tokuyama, Hidetoshi; Fukuyama, Tohru
Journal of the American Chemical Society, 2003 , vol. 125, # 22 p. 6630 - 6631
反应条件
1: 58.3 g / H2 / Pd/C / ethanol / 12 h / 23 °C / 72400.7 Torr
2: 96 percent / pyridine / CH2Cl2 / 0.08 h / 0 °C
View Scheme
参考文献
Yamada, Ken; Kurokawa, Toshiki; Tokuyama, Hidetoshi; Fukuyama, Tohru
Journal of the American Chemical Society, 2003 , vol. 125, # 22 p. 6630 - 6631
反应条件
1: NaNO2; aq. acetic acid / 0 - 23 °C
2: 58.3 g / H2 / Pd/C / ethanol / 12 h / 23 °C / 72400.7 Torr
3: 96 percent / pyridine / CH2Cl2 / 0.08 h / 0 °C
View Scheme
参考文献
Yamada, Ken; Kurokawa, Toshiki; Tokuyama, Hidetoshi; Fukuyama, Tohru
Journal of the American Chemical Society, 2003 , vol. 125, # 22 p. 6630 - 6631
反应条件
magnesium oxide in chloroform; water
参考文献
Fujino; Wakimasu; Mano; Tanaka; Nakajima
Chemical and Pharmaceutical Bulletin, 1976 , vol. 24, # 9 p. 2112 - 2117
反应条件
(i) H2, Pd-C, (ii) /BRN= 509751/, Py; Multistep reaction;
参考文献
Kolodziejczyk,A. et al.
Roczniki Chemii, 1974 , vol. 48, p. 627 - 633
