5,8-二甲氧基-3,4-二氢-1H-2-萘酮合成路线 （共 40 条）
反应条件
5,10,15,20-tetrakis-pentafluorophenyl-21H,23H-porphyrin iron(III) chloride; iodosylbenzene in dichloromethane T=20°C; Further byproducts given;
参考文献
Holland, Herbert L.; Viski, Peter
Journal of Organic Chemistry, 1991 , vol. 56, # 17 p. 5226 - 5229
反应条件
pyridinium chlorochromate in dichloromethane
参考文献
Eli Lilly and Company
Patent: US5026707 A1, 1991 ;
US 5026707 A
反应条件
oxalyl dichloride; dimethyl sulfoxide
参考文献
Manitto, Paolo; Speranza, Giovanna; Monti, Diego; Fontana, Gabriele; Panosetti, Elisa
Tetrahedron, 1995 , vol. 51, # 42 p. 11531 - 11546
反应条件
boron trifluoride diethyl etherate in toluene T=15°C; 0.0833333 h;
参考文献
Perez; Rosell; Mauleon; Carganico
Farmaco, 1991 , vol. 46, # 10 p. 1155 - 1166
反应条件
in dichloromethane; tert-butyl alcohol
参考文献
E. R. Squibb and Sons, Inc.
Patent: US4975461 A1, 1990 ;
反应条件
magnesium bromide in toluene 6 h; Heating;
参考文献
Tririya, Gasirat; Zanger, Murray
Synthetic Communications, 2004 , vol. 34, # 17 p. 3047 - 3059
反应条件
1: petroleum ether 2: sodium ethylate; ethanol 3: ethanol; aqueous HCl View Scheme
参考文献
Tririya, Gasirat; Zanger, Murray
Synthetic Communications, 2004 , vol. 34, # 17 p. 3047 - 3059
反应条件
sulfuric acid T=-5 - 0°C; 2.5 h;
参考文献
Tririya, Gasirat; Zanger, Murray
Synthetic Communications, 2004 , vol. 34, # 17 p. 3047 - 3059
反应条件
titanium(IV) isopropylate; tert.-butylhydroperoxide; L-(+)-DIPT in dichloromethane T=-15°C; 10 h;
参考文献
Rama Rao; Yadav; Bal Reddy; Mehendale
Tetrahedron, 1984 , vol. 40, # 22 p. 4643 - 4647
参考文献
Lewis et al.
Journal of the American Chemical Society, 1952 , vol. 74, p. 5321,5322
