1: 98.7 percent / ammonium carbonate / ethanol; H2O / 1 h / Heating 2: 92 percent / barium hydroxide octahydrate / H2O / 36 h / Heating 3: 94.9 percent / HCl (g) / 24 h / 25 °C View Scheme

1: p-toluenesulfonic acid / benzene / Heating 2: p-toluenesulfonic acid / benzene / 2 h / 80 - 140 °C View Scheme

argentic oxide; nitric acid 1.) dioxane, 2.) room temp., 15 min;

sodium; benzene anschliessendes Behandeln mit CH3I;

T=180°C;

1: 79 percent / tetrahydrofuran / 18 h / Ambient temperature 2: 61 percent / 80percent formic acid / 2 h / 100 - 110 °C View Scheme

1: 79 percent / tetrahydrofuran / 18 h / Ambient temperature 2: 61 percent / 80percent formic acid / 2 h / 100 - 110 °C 3: 93 percent / sodium borohydride / ethanol / 4 h / Ambient temperature 4: tert-butyl hydroperoxide, vanadium oxyacetylacetonate / benzene / 0.75 h / Ambient temperature 5: lithium aluminium hydride / tetrahydrofuran / 4 h 6: 92 percent / triethylamine, sulfur trioxide, pyridine / dimethylsulfoxide / 1 h / Ambient temperature 7: 65 percent / anhyd. AlCl3 / 0.05 h / 180 - 185 °C View Scheme

aluminium trichloride; sodium chloride T=180°C; Friedel-Crafts acylation;

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