1: trimethylsilylacetylene With n-butyllithium in tetrahydrofuran T=0°C; Inert atmosphere; 2: 3β-trimethylsilyloxy-androst-5-ene-17-one in tetrahydrofuran T=20°C;
参考文献
HOLLIS-EDEN PHARMACEUTICALS, INC.
Patent: WO2009/149392 A1, 2009 ;
Location in patent: Page/Page column 13; 14 ;