(S)-2-甲基-1-(4-硝基苯磺酰基)氮丙啶合成路线 （共 3 条）
反应条件
pyridine in dichloromethane T=20°C; 5 h;
参考文献
Crestey, Francois; Witt, Matthias; Frydenvang, Karla; Staerk, Dan; Jaroszewski, Jerzy W.; Franzyk, Henrik
Journal of Organic Chemistry, 2008 , vol. 73, # 9 p. 3566 - 3569
反应条件
N-ethyl-N,N-diisopropylamine in water; ethyl acetate; acetonitrile T=10 - 20°C; 1 h;
参考文献
Farr, Roger N.; Alabaster, Ramon J.; Chung, John Y.L.; Craig, Bridgette; Edwards, John S.; Gibson, Andrew W.; Ho, Guo-Jie; Humphrey, Guy R.; Johnson, Simon A.; Grabowski
Tetrahedron Asymmetry, 2003 , vol. 14, # 22 p. 3503 - 3515
反应条件
1: pyridine / acetonitrile / 3 h / 0 - 10 °C 2: 22.94 kg / diisopropylethylamine / acetonitrile; ethyl acetate; H2O / 1 h / 10 - 20 °C View Scheme
参考文献
Farr, Roger N.; Alabaster, Ramon J.; Chung, John Y.L.; Craig, Bridgette; Edwards, John S.; Gibson, Andrew W.; Ho, Guo-Jie; Humphrey, Guy R.; Johnson, Simon A.; Grabowski
Tetrahedron Asymmetry, 2003 , vol. 14, # 22 p. 3503 - 3515
