1-(环己烯-2-磺酰基)-4-甲苯合成路线 (共 17 条)
反应条件
triphenylphosphine; palladium on activated charcoal in water
T=70°C; 6 h;
参考文献
Felpin, Francois-Xavier; Landais, Yannick
Journal of Organic Chemistry, 2005 , vol. 70, # 16 p. 6441 - 6446
反应条件
bismuth in tetrahydrofuran
1.) r.t., 30 min, 2.) r.t., 4 h;
参考文献
Saikia, Promod; Laskar, Dhrubojyoti D.; Prajapati, Dipak; Sandhu, Jagir S.
Chemistry Letters, 2001 , # 6 p. 512 - 513
反应条件
tetrakis(triphenylphosphine) palladium(0) in tetrahydrofuran; methanol
4 h; Heating;
参考文献
Tsuboyama; Takeda; Torii; Ogura
Chemical and Pharmaceutical Bulletin, 1990 , vol. 38, # 9 p. 2357 - 2363
反应条件
anhydrous iron chloride; chloro-trimethyl-silane in dichloromethane
T=50°C; 12 h;
参考文献
Reddy, M. Amarnath; Reddy, P. Surendra; Sreedhar
Advanced Synthesis and Catalysis, 2010 , vol. 352, # 11-12 p. 1861 - 1869
反应条件
palladium 10 on activated carbon; N-hexadecyl-N,N,N-trimethylammonium bromide; triphenylphosphine in water
T=70°C; Tsuji-Trost Allylation; 3 h; Micellar solutionGreen chemistry;
参考文献
Billamboz, Muriel; Mangin, Floriane; Drillaud, Nicolas; Chevrin-Villette, Carole; Banaszak-Leonard, Estelle; Len, Christophe
Journal of Organic Chemistry, 2014 , vol. 79, # 2 p. 493 - 500
反应条件
1: 73 percent / 4-dimethylaminopyridine / acetone / 24 h / Ambient temperature
2: 75 percent / Pd(Ph3P)4 / tetrahydrofuran; methanol / 4 h / Heating
View Scheme
参考文献
Takeda, Kazuyoshi; Tsuboyama, Kanoko; Torii, Katsumi; Murata, Maki; Ogura, Haruo
Tetrahedron Letters, 1988 , vol. 29, # 33 p. 4105 - 4108
反应条件
dihydrogen peroxide; sodium acetate in acetic acid
T=50°C;
参考文献
Knight, Derek J.; Lin, Peter; Russell, Simon T.; Whitham, Gordon H.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1987 , p. 2701 - 2706
反应条件
acetic acid in chloroform
参考文献
Caglioti,L. et al.
Journal of Organic Chemistry, 1973 , vol. 38, # 5 p. 920 - 923
反应条件
potassium tert-butylate in tetrahydrofuran
参考文献
Arnold, Dennis P.; Burgess-Dean, Leon; Hubbard, Jason; Rahman, M. Abdur
Australian Journal of Chemistry, 1994 , vol. 47, # 5 p. 969 - 974
反应条件
in formamide
T=105°C; 3 h; Yield given. Yields of byproduct given;
参考文献
Knight, Derek J.; Whitham, Gordon H.; Williams, Jonathan G.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1987 , p. 2149 - 2152