2,2,3,3,4,4,4-七氟-1-丁醇合成路线 (共 36 条)
反应条件
carbonylchlorohydrido[bis(2-diphenylphosphinoethyl)amino]ruthenium(II); hydrogen; sodium methylate in methanol T=40°C; P=7500.75 Torr; 23 h; Autoclave; Temperature;
参考文献
Lazzari, Dario; Cassani, Maria Cristina; Bertola, Maurizio; Moreno, Francisco Casado; Torrente, Damiano
RSC Advances, 2013 , vol. 3, # 36 p. 15582 - 15584
反应条件
rhenium; water T=190°C; P=220652 Torr; Hydrogenation;
参考文献
Journal of Organic Chemistry, , vol. 24, p. 1847,1852
反应条件
rhenium T=190°C; P=220652 Torr; Hydrogenation;
参考文献
Journal of Organic Chemistry, , vol. 24, p. 1847,1852
反应条件
in benzene T=30 - 40°C; Abramov reaction; Inert atmosphere;
参考文献
Krutikova; Krutikov; Erkin
Russian Journal of General Chemistry, 2010 , vol. 80, # 3 p. 428 - 433
反应条件
lithium aluminium tetrahydride; diethyl ether
参考文献
US2666797 , ;
Journal of the American Chemical Society, , vol. 74, p. 5422,5425
Journal of the American Chemical Society, , vol. 75, p. 87
US2559749 , ;
反应条件
lithium aluminium tetrahydride in diethyl ether T=0°C;
参考文献
Journal of Medicinal Chemistry, , vol. 56, # 1 p. 73 - 83
参考文献
Journal of the American Chemical Society, , vol. 77, p. 86
反应条件
palladium on activated charcoal; diethyl ether Hydrogenation.an mit Chinolin und Schwefel desaktiviertem Palladium/Kohle; bei anschliessenden Behandlung mit Wasser;
参考文献
Journal of the American Chemical Society, , vol. 74, p. 5422,5425
反应条件
in further solvent(s) reaction in n-butyl ether at -25°C, 11 hours;;
参考文献
Gmelin Handbook: F: PerFHalOrg.4, 2.2.4, page 68 - 115
反应条件
potassium 2,2,2-trifluoroethoxide T=30°C; μ = 0.05 M with potassium trifluoroacetate; Rate constant;
参考文献
Journal of the American Chemical Society, , vol. 115, # 23 p. 10722 - 10727