1,2,3,4-四氯六氟丁烷合成路线 (共 32 条)
反应条件
hydrogen fluoride in tetrachloromethane P=3750.38 - 7500.75 Torr; Autoclave; Product distribution / selectivity;
参考文献
SHOWA DENK K.K.
Patent: US2010/130798 A1, 2010 ;
Location in patent: Page/Page column 5 ;
反应条件
fluorine in CF3OCFClCF2Cl T=10°C;
参考文献
WO2009/87067 A1, ;
Page/Page column 11 ;
参考文献
Industrial and Engineering Chemistry, , vol. 39, p. 402
Chem.Abstr., , p. 7988
反应条件
fluorine; cesium fluoride in CF2ClCF3 T=-80°C; 3 h;
参考文献
EP1457484 A1, ;
Page column 6-7 ;
反应条件
fluorine in 1,1,1,2,2-pentafluoro-2-chlorethyl T=-80°C; 3 h;
参考文献
US2004/199009 A1, ;
Page 3 ;
反应条件
chlorine; fluorine in tetrachloromethane T=40°C; P=5250.53 Torr; AutoclaveInert atmosphere; Product distribution / selectivity;
参考文献
Showa Denko K.K.
Patent: US2010/105968 A1, 2010 ;
Location in patent: Page/Page column 5 ;
反应条件
fluorine T=-80°C; 4 h;
参考文献
US2004/30146 A1, ;
Page 4 ;
反应条件
fluorine T=-100°C; 2 h;
参考文献
US2004/30146 A1, ;
Page 4 ;
反应条件
zinc in dichloromethane; acetic anhydride 2.25 h; Heating;
参考文献
Puy, Michael Van Der; Belter, Randolph K.; Borowski, Ralph J.; Ellis, Lois A. S.; Persichini, Phillip J.; et al.
Journal of Fluorine Chemistry, 1995 , vol. 71, # 1 p. 59 - 64
反应条件
fluorine T=-100 - -80°C; 6.5 h;
参考文献
US2004/30146 A1, ;
Page 3 ;