1,2,3,4-四氯六氟丁烷合成路线 (共 32 条)
反应条件
fluorine T=-107°C; 6.5 h;
参考文献
Journal of the American Chemical Society, , vol. 86, p. 51 - 56
反应条件
acetic anhydride; zinc in dichloromethane T=40°C;
参考文献
Collection of Czechoslovak Chemical Communications, , vol. 73, # 12 p. 1719 - 1728
反应条件
hydrogen fluoride; antimony(V) pentachloride T=160°C; P=29420.3 Torr;
反应条件
acetic anhydride; zinc in dichloromethane T=40°C;
参考文献
Collection of Czechoslovak Chemical Communications, , vol. 73, # 12 p. 1719 - 1728
→
1735-48-41,1,1,2,2,3,4,5,5,6,6,6-十二氟-3,4-二(三氟甲基)己烷
反应条件
in monofluoro-trichloromethane T=-77°C; 8.75 h; Further byproducts given;
参考文献
Journal of the American Chemical Society, , vol. 86, p. 51 - 56
反应条件
acetic anhydride; zinc
参考文献
Journal of the American Chemical Society, , vol. 77, p. 2334
反应条件
zinc in dichloromethane; acetic anhydride Ambient temperature;
参考文献
Journal of Fluorine Chemistry, , vol. 35, p. 421 - 424
反应条件
cadmium in acetonitrile 2 h; Ambient temperature; Further byproducts given;
参考文献
Journal of Fluorine Chemistry, , vol. 36, p. 123 - 140
反应条件
cadmium in acetonitrile 1 h; Ambient temperature;
参考文献
Journal of Fluorine Chemistry, , vol. 36, p. 123 - 140
反应条件
mercury 24 h; Irradiation; Yields of byproduct given;
参考文献
Journal of Fluorine Chemistry, , vol. 55, # 3 p. 271 - 282